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Lead-free coating for shielding X-rays and preparation method of lead-free coating

A lead-free coating, X-ray technology, applied in the field of lead-free coating and its preparation, can solve the problems of hardness, can not meet the needs of social development, toxic texture of radiation protection materials, etc., achieves extensive construction, strong ray absorption ability Effect

Inactive Publication Date: 2019-04-26
上海六晶科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the main anti-radiation materials include anti-radiation lead glass, lead plates, protective doors and various lead protective clothing, etc., but the above-mentioned radiation protection materials are not only poisonous but also hard in texture, and cannot be well pasted on surfaces with curved structures and complex shapes. Effective radiation protection is carried out on the periphery of equipment and instruments, and the development of science is changing with each passing day. From a modern scientific point of view, this material can no longer meet the needs of social development.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0011] Select 1000g alcohol, 20g silane coupling agent, 150g acrylic resin, 850g tungsten powder, 3g anti-settling agent, and 3g defoamer.

[0012] First, modify the metal powder, put 1000g of alcohol in constant temperature water equipment, add 20g of silane coupling agent, mix well, then add the metal powder to make the alcohol submerge the metal powder. Then stir at constant temperature for 2 hours. After the alcohol evaporates, put it into a 100°C oven, take it out after 10 hours, and set it aside.

[0013] Add 150g of acrylic resin to the beaker, add 850g of modified tungsten powder while stirring magnetically, stir magnetically for 6 hours, then add 3g of anti-settling agent and 3g of defoamer, and add diluent to adjust the viscosity according to actual construction conditions.

Embodiment 2

[0015] Select 1000g alcohol, 20g silane coupling agent, 200g acrylic resin, 267g tungsten powder, 533g bismuth powder, 3g anti-settling agent, and 3g defoamer.

[0016] First, modify the metal powder, put 1000g of alcohol in constant temperature water equipment, add 20g of silane coupling agent, mix well, then add the metal powder to make the alcohol submerge the metal powder. Then stir at constant temperature for 2 hours. After the alcohol evaporates, put it into a 100°C oven, take it out after 10 hours, and set it aside.

[0017] Add 200g of acrylic resin into the beaker, add 267g of modified tungsten powder and 533g of modified bismuth powder while stirring magnetically, stir magnetically for 6 hours, then add 3g of anti-settling agent and 3g of defoaming agent, according to actual construction conditions, Add diluent to adjust viscosity.

Embodiment 3

[0019] Select 1000g alcohol, 20g silane coupling agent, 200g acrylic resin, 800g bismuth powder, 3g anti-settling agent, and 3g defoamer.

[0020] First, modify the metal powder, put 1000g of alcohol in constant temperature water equipment, add 20g of silane coupling agent, mix well, then add the metal powder to make the alcohol submerge the metal powder. Then stir at constant temperature for 2 hours. After the alcohol evaporates, put it into a 100°C oven, take it out after 10 hours, and set it aside.

[0021] Add 200g of acrylic resin to the beaker, add 800g of modified bismuth powder while stirring magnetically, stir magnetically for 6 hours, then add 3g of anti-settling agent and 3g of defoamer, and add diluent to adjust the viscosity according to actual construction conditions.

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PUM

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Abstract

The invention relates to the field of shielding coatings, in particular to a lead-free coating for shielding X-rays and a preparation method of the lead-free coating. The lead-free coating comprises raw materials in percentage by mass as follows: raw material A: 0-85wt% of tungsten powder, 0-80wt% of bismuth powder and 15wt%-20wt% of acrylic resin; raw material B: 90wt%-95wt% of alcohol and 5wt%-10wt% of a silane coupling agent; each of the raw material A and the raw material B accounts for 50% of total weight. The preparation process of the lead-free coating comprises the following steps: S1,modifying the tungsten powder and the bismuth powder; S2, adding the acrylic resin to a mixing container, and adding the tungsten powder and the bismuth powder under stirring; S3, adding an anti-settling agent accounting for 1% by mass of the coating and a defoamer accounting for 1% by mass of the coating after stirring is performed for 6 h; S4, adding a dilution regulator for regulating viscosity according to required viscosity. Compared with the prior art, the novel ray shielding coating is prepared from the tungsten powder and the bismuth powder as filling materials and the acrylic resin as a matrix; the coating can meet requirements of the material for non-toxicity, higher ray absorptivity, wide application and convenient construction.

Description

technical field [0001] The invention relates to the field of shielding coatings, in particular to a lead-free coating for shielding X-rays and a preparation method thereof. Background technique [0002] Since the discovery of X-rays in 1895, natural radioactivity in 1896, artificial radioactivity in 1934, and nuclear fission in 1938, ionizing radiation has been widely used in various industries, agriculture, medical and health institutions, education, research institutions, and nuclear fuel cycle facilities. application and rapid development. In particular, X-ray imaging technology has become an indispensable and important part of modern medicine, and X-rays provide indispensable application value for clinical diagnosis. As we all know, X-rays have a strong penetrability to human tissues, and the penetrating ability to tissues of different densities is different. Therefore, through X-rays, images of human tissue with different levels of black and white can be displayed, an...

Claims

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Application Information

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IPC IPC(8): C09D133/00C09D5/32C09D7/62
CPCC08K2003/0837C08K2003/0887C09D5/32C09D7/62C09D133/00C08K9/06C08K3/08
Inventor 吴敏张静朱玉斌
Owner 上海六晶科技股份有限公司
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