A kind of tobacco extract concentration process
A tobacco extract and extract technology, applied in ultrafiltration, membrane technology, chemical instruments and methods, etc., can solve problems such as difficult cleaning and reverse osmosis membrane pollution, and achieve easy cleaning, light membrane pollution, and high concentration Effect
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Embodiment 1
[0043] A process for concentrating tobacco extract, comprising the steps of:
[0044] Step (1), primary purification: removing impurities from the tobacco extract to obtain a tobacco primary purification extract with a suspended matter content of 1-1.5%;
[0045] Step (2), microfiltration filtration: use a membrane with a pore size of 400nm to perform microfiltration on the tobacco primary purification extract obtained in step (1) at 90-100°C. During microfiltration, the operating pressure rises to 0.3MPa, and the filtration is stopped , to obtain retentate and permeate;
[0046] Step (3), forward osmosis concentration: performing forward osmosis concentration on the permeate obtained in step (2), to obtain tobacco extract concentrate and diluted drawing solution;
[0047] The extraction agent used in the concentration process is NaCl; the concentration temperature is 5-20°C, and the pressure is 0.1-0.3MPa; the concentration adopts a single-stage concentration method; the mem...
Embodiment 2
[0050] A process for concentrating tobacco extract, comprising the steps of:
[0051] Step (1), primary purification: remove impurities from the extract obtained by solid-liquid separation after extraction of tobacco raw materials, and obtain a tobacco primary purification extract with a suspended matter content of 1.8-3%; the method of removing impurities is natural sedimentation;
[0052] Step (2), microfiltration filtration: use a ceramic membrane with a pore size of 50nm to perform microfiltration on the tobacco primary purification extract obtained in step (1) at 10-20°C. During microfiltration, the operating pressure rises to 0.3MPa and stops Filter to obtain retentate and permeate;
[0053] Step (3), forward osmosis concentration: performing forward osmosis concentration on the permeate obtained in step (2), to obtain tobacco extract concentrate and diluted drawing solution;
[0054] The extraction agent used in the concentration process is potassium citrate; the conce...
Embodiment 3
[0057] A process for concentrating tobacco extract, comprising the steps of:
[0058] Step (1), primary purification: remove impurities from the extract obtained by solid-liquid separation after extraction of tobacco raw materials, and obtain a tobacco primary purification extract with a suspended matter content of 1.8-2.5%; the method of removing impurities is decanter centrifugation;
[0059] Step (2), microfiltration filtration: the tobacco primary purification extract obtained in step (1) is subjected to microfiltration at 0-40°C using a polyvinylidene fluoride membrane with a pore size of 200nm. During microfiltration, the operating pressure rises to 0.3MPa, stop filtering to obtain retentate and permeate;
[0060] Step (3), forward osmosis concentration: the permeate obtained in step (2) is subjected to forward osmosis concentration to obtain tobacco extract concentrate and diluted drawing solution; the membrane used for forward osmosis concentration is cellulose acetate...
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