Chinlon 6 short fiber having cool feeling and preparation method thereof
A technology of short fiber and cool feeling, which is applied in the field of cool feeling nylon 6 short fiber and its preparation. It can solve the problems of affecting fibers, poor air permeability, and disappearing cool feeling of products, and achieves the effect of improving cool feeling and improving dispersion uniformity
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Embodiment 1
[0045] A kind of preparation method of cool feeling nylon 6 staple fiber, concrete steps are as follows:
[0046] (1) prepare mixture;
[0047] (1.1) Pretreatment of cooling functional powder;
[0048] First, disperse the cooling functional powder with a particle size of 12-32nm in absolute ethanol to obtain a suspension with a solid content of 13wt%, then put the suspension into a grinder and grind it for 2.5 hours, and then add caprolactam sodium salt Grinding at 55°C for 1 hour, and finally after 4 hours of slurry aging, drying and jet milling to obtain the pretreated cooling function powder, wherein the cooling function powder refers to mica and jade with a mass ratio of 1:1 The compounded powder has a thermal conductivity of 1.55W / m·K, and the surface of the cool-feeling functional powder is coated with caprolactam sodium salt;
[0049] (1.2) mixing;
[0050] First, put the pretreated cool-feeling functional powder in the melt of caprolactam and heptadecane, then mecha...
Embodiment 2
[0056] A kind of preparation method of cool feeling nylon 6 staple fiber, concrete steps are as follows:
[0057] (1) prepare mixture;
[0058] (1.1) Pretreatment of cooling functional powder;
[0059] First, disperse the cooling functional powder with a particle size of 30-55nm in absolute ethanol to obtain a suspension with a solid content of 18wt%, then put the suspension into a grinder and grind it for 2 hours, and then add caprolactam magnesium bromide Grinding at 50°C for 1 hour, and finally after 11 hours of slurry aging, drying and jet milling to obtain the pretreated cooling function powder, wherein the cooling function powder refers to jade and Tai Chi with a mass ratio of 1:2 The thermal conductivity of the powder compounded with stone is 1.6W / m·K, and the surface of the cooling functional powder is coated with caprolactam magnesium bromide;
[0060] (1.2) mixing;
[0061] First, place the pretreated cooling functional powder in the melt of caprolactam and octade...
Embodiment 3
[0067] A kind of preparation method of cool feeling nylon 6 staple fiber, concrete steps are as follows:
[0068] (1) prepare mixture;
[0069] (1.1) Pretreatment of cooling functional powder;
[0070] First, disperse the cooling functional powder with a particle size of 5.8-12.5nm in absolute ethanol to obtain a suspension with a solid content of 10wt%, then add the suspension to a grinder for grinding for 3 hours, and then add Grignard reagent Grinding at 80°C for 2.5 hours, and finally after 5 hours of slurry aging, drying and airflow pulverization to obtain the pretreated cooling function powder, wherein the cooling function powder refers to the mass ratio of 1:1 mica and The thermal conductivity of Taichi stone is 1.2W / m·K. The surface of the cooling powder is coated with Grignard reagent, which is a commercially available alkylmagnesium halide organic compound;
[0071] (1.2) mixing;
[0072] First, place the pretreated cooling functional powder in a mixture of heptad...
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