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Stain-resistant nanometer garment fabric and preparation method thereof

A nano-technology, anti-fouling technology, applied in the field of clothing fabrics, can solve the problems of reduced anti-fouling performance, reduced anti-fouling performance, etc., to achieve the effect of improving anti-fouling ability, high hydrophobic anti-fouling performance, and achieving anti-fouling performance

Inactive Publication Date: 2019-03-01
江阴市伊芙特制衣有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Sodium borate is added in the process of preparing the composite fiber in the present invention, and the sodium borate has a certain bonding performance. After being fixed by crosslinking, the titanium / silica sol is firmly combined on the surface of the acetate fiber, preventing the peeling of the sol layer on the fiber surface during the washing process. Reduce its stain resistance and solve the problem of lower stain resistance of existing fabrics under long-term washing

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Stain-resistant nanometer garment fabric and preparation method thereof
  • Stain-resistant nanometer garment fabric and preparation method thereof
  • Stain-resistant nanometer garment fabric and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] The specific preparation process of composite blended cellulose acetate is as follows:

[0034] Step 1: Add 1kg of γ-(2,3-glycidoxy)propyltrimethoxysilane and 10L of absolute ethanol into the reaction vessel, raise the temperature to 60°C for reflux reaction for 2 hours, and add hydrochloric acid to it at the same time to control the concentration of the reaction solution. pH=2, obtain silica gel solution;

[0035] Step 2: Dissolve 1kg of cellulose acetate in 10L of acetone, add the dissolved cellulose acetate solution into the reaction vessel, add 5.6kg of silica colloid solution and 0.3kg of dibutyltin dilaurate to it at the same time, stir and mix and heat up to 70°C , then add 0.61kg tetrabutyl titanate to the reaction vessel, and add hydrochloric acid therein to adjust the pH=3 of the solution, control the temperature to keep the reflux reaction for 4-5h, and obtain a viscous composite fiber colloid solution;

[0036] Step 3: Pour the viscous composite fiber collo...

Embodiment 2

[0043] The specific preparation process of composite blended cellulose acetate is as follows:

[0044] Step 1: Add 1kg of γ-(2,3-glycidoxy)propyltrimethoxysilane and 12L of absolute ethanol into the reaction vessel, raise the temperature to 60°C for reflux reaction for 2 hours, and add hydrochloric acid to it at the same time to control the concentration of the reaction solution. pH=2, obtain silica gel solution;

[0045] Step 2: Dissolve 1kg of cellulose acetate in 10L of acetone, add the dissolved cellulose acetate solution into the reaction vessel, add 5.8kg of silica colloid solution and 0.3kg of dibutyltin dilaurate to it at the same time, stir and mix, then heat up to 70°C , then add 0.63kg tetrabutyl titanate to the reaction vessel, and add hydrochloric acid therein to adjust the pH=3 of the solution, control the temperature to keep the reflux reaction for 4-5h, and obtain a viscous composite fiber colloid solution;

[0046] Step 3: Pour the viscous composite fiber col...

Embodiment 3

[0053] The specific preparation process of composite blended cellulose acetate is as follows:

[0054] Step 1: Add 1kg of γ-(2,3-glycidoxy)propyltrimethoxysilane and 10L of absolute ethanol into the reaction vessel, raise the temperature to 60°C for reflux reaction for 2 hours, and add hydrochloric acid to it at the same time to control the concentration of the reaction solution. pH=2, obtain silica gel solution;

[0055] Step 2: Dissolve 1kg of cellulose acetate in 10L of acetone, add the dissolved cellulose acetate solution into the reaction vessel, add 3.5kg of silica colloid solution and 0.3kg of dibutyltin dilaurate to it at the same time, stir and mix, then heat up to 70°C , then add 0.41kg tetrabutyl titanate to the reaction vessel, and add hydrochloric acid therein to adjust the pH=3 of the solution, control the temperature to keep the reflux reaction for 4-5h, and obtain a viscous composite fiber colloid solution;

[0056] Step 3: Pour the viscous composite fiber col...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention discloses a preparation method of a stain-resistant nanometer garment fabric. The specific preparation process comprises the following steps: adding complex blended cellulose acetate fibers and modified polyurethane fibers to acetone, wherein the complex blended cellulose acetate fibers and the modified polyurethane fibers are dissolved in acetone, carrying out heating to 80 DEG C, carrying out stirring for dissolving, adding sodium borate, adding hydrochloric acid, adjusting the pH of the solution to be 2, carrying out constant-temperature reflux reaction for 6-7 h, carrying outheating to 90 DEG C, adding trifluoroacetic anhydride, carrying out constant-temperature stirring reaction for 5h, carrying out evaporation to obtain solid substance, and carrying out washing and drying, thus obtaining complex solid fibers; and adding the complex solid fibers to a melt spinning machine for spinning, spinning the fiber filaments to form complex yarns, and weaving the complex yarns, thus obtaining the stain-resistant fabric. In the preparation process of the complex fibers, sodium borate is added, sodium borate has certain bonding property, after crosslinking and fixing, titanium / silica sol is firmly boned to the surfaces of the cellulose acetate fibers, and thus the phenomenon that during the washing process, the sol layers on the surfaces of the fibers is stripped, consequently, the stain-resisting property is reduced is avoided.

Description

technical field [0001] The invention belongs to the field of clothing fabrics, and relates to a stain-resistant nano clothing fabric and a preparation method thereof. Background technique [0002] With the improvement of people's living standards, there are higher requirements for the quality of clothes. For those who work in dirty oil-stained factories or auto repair companies for a long time, the stain resistance and tensile wear resistance of clothes have certain The existing stain-resistant fabrics usually bond nano-titanium dioxide in the fabric, and realize the stain-resistant performance of the fabric through the action of nano-titanium dioxide. At the same time, the high stain resistance of the fabric cannot be achieved only through the effect of titanium dioxide, and the stain resistance cannot be fully realized for the oil stains penetrating in the gaps of the fabric. The content of nano-titanium dioxide is reduced, which in turn reduces its oil resistance. Cont...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A41D31/00D01F1/10D01F2/28D01F6/94
CPCA41D31/00D01F1/10D01F2/28D01F6/94
Inventor 蔡阳铎林惠英
Owner 江阴市伊芙特制衣有限公司
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