Metal-doped calcium zirconate material, and preparation method and use thereof
A calcium zirconate and metal technology, applied in the field of calcium zirconate materials, can solve problems such as high cost, poor mechanical properties and stability, and high price, and achieve low cost, stable physical and chemical properties, and good stability.
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Embodiment 1
[0027] This embodiment provides a method for preparing a metal-doped calcium zirconate material, which specifically includes the following steps:
[0028] S1, calcium carbonate (CaCO 3 ) powder, zirconia (ZrO 2 ) powder and iron oxide (Fe 2 o 3 ) powder in molar ratio, CaCO 3 :ZrO 2 :Fe 2 o 3 =1:0.7:0.15 for batching. Among them, CaCO 3 The analytical purity of the powder is 99%, ZrO 2 The powder is analytically pure with a purity of 99%, Fe 2 o 3 The analytical purity of the powder was 99.9%.
[0029] S2. Mix all the powders obtained in step S1 together and put them into an agate mortar for grinding for 2 hours to form the first material to be molded. The particle size of the first material to be molded is ≤100 μm.
[0030] Specifically, using an agate mortar for grinding has simple operation and low cost, and avoids the need to add some reagents when grinding in other ways, which may lead to the introduction of impurities or increase the experiment time. Mixing ...
Embodiment 2
[0049] This embodiment provides a method for preparing a metal-doped calcium zirconate material, which specifically includes the following steps:
[0050] S1, calcium carbonate (CaCO 3 ) powder, zirconia (ZrO 2 ) powder and iron oxide (Fe 2 o 3 ) powder in molar ratio, CaCO 3 :ZrO 2 :Fe 2 o 3 =1:0.9:0.05 for batching. Among them, CaCO 3 The analytical purity of the powder is 99%, ZrO 2 The powder is analytically pure with a purity of 99%, Fe 2 o 3 The analytical purity of the powder was 99.9%.
[0051] S2. Mix all the powders obtained in step S1 and put them into an agate mortar for grinding for 1.5 hours to form the first material to be molded. The particle size of the first material to be molded is ≤100 μm.
[0052] S3. Compress the first material to be molded under a compression pressure of 6 MPa by cold pressing, and then perform calcination at 1000° C. for 8 hours to obtain iron-doped calcium zirconate composites. The composition of the obtained complex is Ca...
Embodiment 3
[0059] This embodiment provides a method for preparing a metal-doped calcium zirconate material, which specifically includes the following steps:
[0060] S1, calcium carbonate (CaCO 3 ) powder, zirconia (ZrO 2 ) powder and iron oxide (Fe 2 o 3 ) powder in molar ratio, CaCO 3 :ZrO 2 :Fe 2 o 3 =1:0.8:0.1 for batching. Among them, CaCO 3 The analytical purity of the powder is 99%, ZrO 2 The powder is analytically pure with a purity of 99%, Fe 2 o 3 The analytical purity of the powder was 99.9%.
[0061] S2. Mix all the powders obtained in step S1 together and put them into an agate mortar for grinding for 3 hours to form the first material to be molded. The particle size of the first molded material is ≤100 μm.
[0062] S3. Compress the first material to be molded under a compression pressure of 10 MPa by cold pressing, and then perform calcination at 1200° C. for 4 hours to obtain an iron-doped calcium zirconate composite. The composition of the obtained complex is...
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