Fruit and vegetable washing agent
A technology for fruit and vegetable detergents and auxiliaries, which is applied in the direction of detergent compositions, detergent compounding agents, surface active detergent compositions, etc., can solve the problems of not being able to remove pesticide residues and heavy metal pollution components in fruits and vegetables, and achieve Excellent physiological inertia and biocompatibility, easy to use and clean, easy to clean effect
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[0025] The preparation method of composite mercapto-containing microcapsules comprises the following steps:
[0026] (1) Mix mercaptobenzoic acid and N,N-dimethylformamide according to the mass ratio of 1:15~25, adjust the pH to 4.6~5.2 with HCl solution with a concentration of 0.1mol / L, protect with nitrogen, and use 300~ 450r / min magnetic stirring for 25~50min to get the premixed solution, take the premixed solution and add dopamine hydrochloride and N-hydroxysuccinimide at a mass ratio of 5~8:2~5:1 to mix, seal at room temperature and keep away from light for 6~8h , to obtain the pretreated product, take the pretreated chitosan solution and add the pretreated product in a mass ratio of 4~8:1~3 to mix, stir magnetically at 300~500r / min for 30~50min, and use NaOH solution with a concentration of 0.1mol / L Adjust the pH to 8.6~9.2, let stand for 8~12h, dialyze with 50% ethanol solution for 3~5 days, take the dialyzate and freeze-dry it at -60℃ to obtain the dried product;
[0...
Embodiment 1
[0031] Pretreatment rice washing water: in parts by mass, take 5 parts of rice and 30 parts of water and mix them for rice washing operation to obtain primary washing water, take palygorskite and pulverize through a 120-mesh sieve, and take the sieved particles according to the mass ratio of 1: 4 Add PBS buffer solution with a pH of 6.2 to mix, stir at 300r / min for 20min, let stand for 1h, filter, take out, add the filter residue to primary washing water at a mass ratio of 1:4, evaporate under reduced pressure, and concentrate in vacuo to 30% of the original volume , that is, the pretreated rice washing water is obtained.
[0032] Surfactant: mix lauryl dimethyl betaine and sodium lauryl sulfate at a mass ratio of 4:1 to obtain a surfactant.
[0033] Auxiliary: Mix NaCl, potassium sulfide, and sodium citrate at a mass ratio of 4:1:1 to obtain the auxiliary.
[0034] Auxiliary liquid: Mix Ɛ-polylysine and sodium citrate solution at a mass ratio of 1:4 to obtain the auxiliary l...
Embodiment 2
[0042] Pretreatment rice washing water: in parts by mass, take 7 parts of rice and 35 parts of water and mix them for rice washing operation to obtain primary washing water, take palygorskite and pulverize through a 120-mesh sieve, and take the sieved particles according to the mass ratio of 1: 5 Add PBS buffer solution with a pH of 6.4 and mix, stir at 350r / min for 20~45min, let it stand for 2h, filter, take, add the filter residue according to the mass ratio of 1:6, add primary washing water, evaporate under reduced pressure, and concentrate in vacuo to the original volume 35%, that is, the pretreated rice water.
[0043] Surfactant: mix lauryl dimethyl betaine and sodium lauryl sulfate at a mass ratio of 4:1.5 to obtain a surfactant.
[0044] Auxiliary: Mix NaCl, potassium sulfide, and sodium citrate at a mass ratio of 4:1:1.5 to obtain the auxiliary.
[0045] Auxiliary liquid: Mix Ɛ-polylysine and sodium citrate solution at a mass ratio of 1:6 to obtain the auxiliary liqu...
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