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M-diamide compound, and preparation method and application of compound

A compound and diamide technology, which is applied to the field of meta-diamide compounds and their preparation, can solve the problems of reducing the effect of pharmaceutical agents, and achieve the effects of less drug residues, fast onset of action, and environmental protection.

Inactive Publication Date: 2018-09-28
SHANGHAI TAIHE INT TRADE CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Since pests are very prone to drug resistance, which will lead to the reduction of the effect of many agents, it is still necessary to actively develop new insecticides with fast-acting and high insecticidal activity at low doses in this field to meet the needs of agriculture and forestry.

Method used

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  • M-diamide compound, and preparation method and application of compound
  • M-diamide compound, and preparation method and application of compound
  • M-diamide compound, and preparation method and application of compound

Examples

Experimental program
Comparison scheme
Effect test

preparation Embodiment 1

[0305] In this example, compound 2 of the present invention was used as a representative compound to prepare preparations, as follows:

[0306] Evenly mix 30 parts of the compound 2 of the present invention, 15 parts of polyoxyethylene styryl phenyl ether, 10 parts of phosphorous acid, and 45 parts of xylene to obtain an emulsifiable concentrate with a concentration of 30% of the compound 2 of the present invention.

preparation Embodiment 2

[0308] In this example, compound 7 of the present invention was used as a representative compound to prepare preparations, as follows:

[0309] Stir and mix 20 parts of compound 7 of the present invention, 2 parts of sodium lauryl sulfate, 2 parts of dialkyl sulfosuccinate, 1 part of β-naphthalenesulfonic acid formaldehyde condensate sodium salt, 75 parts of diatomaceous earth, A 20% wettable powder of compound 7 of the present invention was obtained.

preparation Embodiment 3

[0311] In this example, compound 5 of the present invention was used as a representative compound to prepare preparations, as follows:

[0312] 30 parts of compound 5 of the present invention, 10 parts of ethylene glycol, 6 parts of nonylphenol polyethylene glycol ether, 10 parts of sodium lignosulfonate, 10 parts of carboxymethyl cellulose, 1 part of silicone oil aqueous solution, and water to 100 %, to obtain a 30% suspension concentrate of compound 5 of the present invention.

[0313] Example of biological activity test

[0314] Various pests were tested using the compounds of the present invention obtained above.

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PUM

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Abstract

The invention provides a m-diamide compound, and a preparation method and application of the compound. The m-diamide compound has a structure shown as formula I. The m-diamide compound can have high insecticidal activity at a low dose, takes effect quickly, can exert the insecticidal activity a day after application and achieve the very high insecticidal activity within 3 days, and has good quickaction performance; in addition, since the compound has a good effect at the low dose, harms to plants and human due to excessive concentration are reduced; the residue is low during application; theenvironmental protection is better facilitated; and the preparation method of the compound is simple, efficient, easy in large-scale production and wide in application prospect.

Description

technical field [0001] The invention belongs to the field of insecticides, and relates to a meta-diamide compound and a preparation method and application thereof. Background technique [0002] In the production of crops such as agriculture and horticulture, the damage caused by pests is still very significant. Due to the resistance of pests to existing pesticides and the unfriendly environment of existing pesticides, it is always necessary to develop better activity and lower dosage. , New insecticides that are more environmentally friendly. [0003] The insecticidal activity of intermediate diamide compounds has been reported, such as CN102119143A discloses compound KC1 (i.e. compound 7-1574 in CN102119143A), KC2 (i.e. compound 7-1595 in CN102119143A) and KC3 (i.e. compound 6-5907 in CN102119143A) And its insecticidal activity, among which KC2 has been commercialized, and its English common name is broflanilide. These disclosed compounds have insecticidal activity, howev...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07C237/42C07C255/50C07D271/06A01N37/18A01N37/34A01N43/836A01P7/04
CPCA01N37/18A01N37/34A01N43/82C07C237/42C07C255/50C07D271/06C07C2601/02C07C233/88C07C255/57A01N37/46A01N37/48A01N41/10
Inventor 吕亮刘吉永相君成马文静周丽淇侯爽倪珏萍李宗成
Owner SHANGHAI TAIHE INT TRADE CO LTD
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