Liquid storage antibacterial material and preparation method thereof as well as liquid storage antibacterial cup
An antibacterial material and antibacterial cup technology, applied in the field of medical devices, can solve the problems of difficult storage of body fluids, inaccurate measurement, and inconvenient retention of liquid storage vessels, and achieve the effects of optimizing antibacterial properties, avoiding poor dispersion, and optimizing production processes.
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Embodiment 1
[0051] The preparation method of the liquid storage antibacterial material of the embodiment of the present invention comprises:
[0052] (1) Add zeolite to 18wt% NH at a solid-to-liquid ratio of 1:8g / mL 4 In Cl solution, soak for 6 hours at 50°C, clarify, remove the supernatant, and then add an equal volume of NH 4 The Cl solution was soaked at 95 °C for 1 h, and the filter residue was washed with distilled water after suction filtration, and the filter residue was dried at 100 °C to obtain NH 4+ type zeolite;
[0053] (2) NH 4+ Type zeolite was added to the Cu-containing 2+ and Zn 2+ In the mixed solution, react at a constant temperature at 20°C for 12h, and wash with deionized water after suction filtration until there is no Cu 2+ Filter out to obtain the zeolite antibacterial agent;
[0054] (3) Mix and melt the zeolite antibacterial agent, polypropylene and grafted polypropylene at a weight ratio of 2:1:0.5 at 150-250°C, extrude the spline in the extruder, and pelle...
Embodiment 2
[0060] The preparation method of the liquid storage antibacterial material of the embodiment of the present invention comprises:
[0061] (1) Add zeolite to 22wt% NH at a solid-to-liquid ratio of 1:12g / mL 4 In Cl solution, soak for 5 hours at 80°C, clarify, remove the supernatant, and then add an equal volume of NH 4 Digest the Cl solution at 100°C for 2 hours, wash the filter residue with distilled water after suction filtration, and dry the filter residue at 110°C to obtain NH 4+ type zeolite;
[0062] (2) NH 4+ Type zeolite was added to the Cu-containing 2+ and Zn 2+ In the mixed solution, react at a constant temperature at 80°C for 2h, and wash with deionized water after suction filtration until there is no Cu 2+ Filter out to obtain the zeolite antibacterial agent;
[0063] (3) Mix and melt the zeolite antibacterial agent, polypropylene and grafted polypropylene at a weight ratio of 2:1.2:0.7 at 150-250°C, extrude the splines in the extruder, and cut into pellets af...
Embodiment 3
[0069] The preparation method of the liquid storage antibacterial material of the embodiment of the present invention comprises:
[0070] (1) Add zeolite to 20wt% NH at a solid-to-liquid ratio of 1:10g / mL 4 In Cl solution, soak for 8 hours at 60°C, clarify, remove the supernatant, and then add an equal volume of NH 4 The Cl solution was soaked at 105°C for 1.5h, the filter residue was washed with distilled water after suction filtration, and the filter residue was dried at 105°C to obtain NH 4+ type zeolite;
[0071] (2) NH 4+ Type zeolite was added to the Cu-containing 2+ and Zn 2+ In the mixed solution, react at a constant temperature of 60 ° C for 4 h, and wash with deionized water after suction filtration until there is no Cu 2+ Filter out to obtain the zeolite antibacterial agent;
[0072] (3) Mix and melt the zeolite antibacterial agent, polypropylene and grafted polypropylene at 200°C according to the weight ratio of 5:3:1.5, extrude the sample in the extruder, an...
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