PPR plastic pipe with self-repairing function and preparation method thereof
A plastic pipe and self-repair technology, which is applied in the field of PPR plastic pipe and its preparation, can solve the problems of manual repair of PPR pipe, manual repair, waste of manpower, etc., and achieve the effects of preventing pipe burst, prolonging service life and short reaction time
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Embodiment 1
[0039] Example 1 Preparation of PPR plastic pipe with self-repair function
[0040] (1) Preparation of self-repairing microcapsules
[0041] Ⅰ. Mix urea and formaldehyde in a stirring environment. The weight ratio of urea to formaldehyde is 1:1.5. After the urea is completely dissolved, the pH of the reaction system is adjusted to 8.5 with sodium hydroxide, heated to 70°C, and reacted for 1.5 hours to obtain Urea-formaldehyde resin prepolymer;
[0042] Ⅱ. Add emulsifier, resorcinol and cyclopentadiene to the urea-formaldehyde resin prepolymer obtained above, and disperse it at 500r / min for 20min to form a stable oil-in-water emulsion;
[0043] Ⅲ. Then adjust the pH of the reaction system to 4~5 with dilute hydrochloric acid, heat up to 65°C, react for 2.5h, cool to room temperature, filter with suction, and dry to obtain self-repairing microcapsules.
[0044] (2) Preparation of PPR plastic pipe with self-repair function
[0045] a. Mix 1 part by weight of polyacrylic acid and 1.2 parts ...
Embodiment 2
[0047] Example 2 Preparation of PPR plastic pipe with self-repair function
[0048] (1) Preparation of self-repairing microcapsules
[0049] Ⅰ. Mix urea and formaldehyde in a stirring environment. The weight ratio of urea to formaldehyde is 1:1.8. After the urea is completely dissolved, adjust the pH of the reaction system to 8-9 with sodium hydroxide, heat up to 72°C, and react for 1.8h , Get urea-formaldehyde resin prepolymer;
[0050] Ⅱ. Add emulsifier, resorcinol and cyclopentadiene to the urea-formaldehyde resin prepolymer obtained above, and disperse it at 500r / min for 20min to form a stable oil-in-water emulsion;
[0051] Ⅲ. Then adjust the pH of the reaction system to 4~5 with dilute hydrochloric acid, heat up to 68°C, react for 2.8 hours, cool to room temperature, filter and wash with suction, and dry to obtain self-repairing microcapsules.
[0052] (2) Preparation of PPR plastic pipe with self-repair function
[0053] a. Mix 1 part by weight of polyacrylic acid and 1.2 parts b...
Embodiment 3
[0055] Example 3 Preparation of PPR plastic pipe with self-repair function
[0056] (1) Preparation of self-repairing microcapsules
[0057] Ⅰ. Mix urea and formaldehyde in a stirring environment. The weight ratio of urea to formaldehyde is 1:1.2. After the urea is completely dissolved, adjust the pH of the reaction system to 8-9 with sodium hydroxide, heat up to 68°C, and react for 1.2h , Get urea-formaldehyde resin prepolymer;
[0058] Ⅱ. Add emulsifier, resorcinol and cyclopentadiene to the urea-formaldehyde resin prepolymer obtained above, and disperse it at 500r / min for 20min to form a stable oil-in-water emulsion;
[0059] Ⅲ. Then adjust the pH of the reaction system to 4~5 with dilute hydrochloric acid, heat up to 68°C, react for 2.5 hours, cool to room temperature, filter with suction, and dry to obtain self-repairing microcapsules.
[0060] (2) Preparation of PPR plastic pipe with self-repair function
[0061] a. Mix 1 part by weight of polyacrylic acid and 1.1 parts by weight ...
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