Sweet food additive for drinks and preparation method
A technology for food additives and sweetness, which is applied in the directions of food ingredients containing non-sugar sweeteners, food ingredients as taste improvers, food ingredients, etc., and can solve the problems of low biological stability, high calorie disease, and low cost. , to achieve the effect of simple preparation process, long duration of sweet taste and long time
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Embodiment 1
[0040](1) Add neohesperidin, ring-opening agent sodium hydroxide and deionized water into the reaction container, stir to promote dissolution, add palladium carbon catalyst, seal the container, and replace the air in the container with nitrogen; while continuing Stir while feeding hydrogen to replace the nitrogen in the container; the reaction time is 12 hours, after the reaction is completed, feed nitrogen to replace the hydrogen in the container, and then stop the reaction to obtain a solution of neohesperidin dihydrochalcone; wherein, neohesperidin dihydrochalcone Hesperidin is 10 parts by weight, 5 parts by weight of ring opener, 83 parts by weight of deionized water, and 2 parts by weight of palladium carbon catalyst;
[0041] (2) Add glycyrrhizin sweetener to the neohesperidin dihydrochalcone solution in step (1), stir and mix evenly, heat to evaporate and remove the water part, and obtain glycyrrhizin with a mass concentration of 60%. A mixed solution of neohesperidin d...
Embodiment 2
[0045] (1) Add neohesperidin, ring-opening agent and deionized water into the reaction container, stir to promote dissolution, add palladium carbon catalyst, seal the container, and replace the air in the container with nitrogen gas; while continuing to stir, Pass in hydrogen to replace the nitrogen in the container; after the reaction is over, pass in nitrogen to replace the hydrogen in the container, and then stop the reaction to obtain neohesperidin dihydrochalcone solution; the ring-opening agent is sodium hydroxide; palladium carbon catalyst The content of palladium powder in the medium is 5%; wherein 8 parts by weight of neohesperidin, 8 parts by weight of ring opener, 83 parts by weight of deionized water, and 1 part by weight of palladium carbon catalyst; the stirring speed is 500r / min, and the reaction time is 12h;
[0046] (2) Add glycyrrhizin sweetener to the neohesperidin dihydrochalcone solution in step (1), stir and mix evenly, heat to evaporate and remove the wat...
Embodiment 3
[0050] (1) Add neohesperidin, ring-opening agent and deionized water into the reaction container, stir to promote dissolution, add palladium carbon catalyst, seal the container, and replace the air in the container with nitrogen gas; while continuing to stir, Pass in hydrogen to replace the nitrogen in the container; after the reaction is over, pass in nitrogen to replace the hydrogen in the container, and then stop the reaction to obtain neohesperidin dihydrochalcone solution; the ring-opening agent is sodium hydroxide; palladium carbon catalyst The content of palladium powder in the medium is 6%; 8 parts by weight of neohesperidin, 5 parts by weight of ring opener, 86 parts by weight of deionized water, and 1 part by weight of palladium carbon catalyst; the stirring speed is 600r / min, and the reaction time is 11h;
[0051] (2) Add glycyrrhizin sweetener to the neohesperidin dihydrochalcone solution in step (1), stir and mix evenly, heat to evaporate and remove the water part,...
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