Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Online detecting method of content of heavy metal in water

A detection method and heavy metal technology, applied in the preparation of test samples, measurement of color/spectral characteristics, material analysis through observation of the influence of chemical indicators, etc., can solve the problems of reducing detection efficiency and achieve improved detection efficiency, Real-time online detection and the effect of reducing work intensity

Inactive Publication Date: 2018-03-06
苏州泰坤检测技术有限公司
View PDF4 Cites 2 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] This requires us to detect heavy metals in water, especially manganese, copper and iron, and the existing water sample detection devices, when detecting manganese, copper and iron, respectively react under the corresponding reagent conditions, and cooperate with them after complete reaction. Other reagents are used for detection, and each reagent is operated separately during the reaction process, and the detection efficiency is reduced by changing tubes for multiple detection

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] Embodiment 1: the heavy metal is copper, and in the S2, the reagent added to the original water sample of the digestion device is a mixed solution of sulfuric acid and nitric acid; heated together until the temperature reaches 120°C, and digested in an acidic environment for 1-10min, Obtain a completely dissolved drug-dosed water sample, adjust the pH to neutral after cooling, add citrate as a masking agent to eliminate interference, add a buffer solution until alkaline, and then add a color developer.

Embodiment 2

[0039] Embodiment 2: Similar in structure to Embodiment 1, the difference is: the heavy metal is iron, and in the S2, the reagent added to the original water sample of the digestion device is hydroxylamine hydrochloride. After the reaction is complete, adjust the pH to 5. Add color developer.

Embodiment 3

[0040] Embodiment 3: Similar to the structure of Embodiment 1, the difference is that: the heavy metal is manganese, and in the S2, the reagent added to the original water sample of the digestion device is a mixed solution of mercuric sulfate-phosphoric acid, and it is combined Heat until the temperature reaches 60°C-70°C, digest in an acidic environment for 1min, and after cooling, a completely dissolved drug-dosed water sample is obtained.

[0041] Compared with the prior art, the beneficial effects of the online detection method of the present invention are mainly reflected in: the automatic control operation of heavy metal content detection is realized, which is convenient for rapid sampling detection; and online detection can be performed in real time to realize wireless transmission and control of detection data, Improve work efficiency and reduce work intensity.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses an online detecting method of the content of heavy metal in water. The online detecting method comprises the following steps: sucking an original water sample of a river channel into a storage cabin by a sampling device, and switching off a water inlet valve and switching on a water outlet valve when a liquid level sensor in the storage cabin induces that the water sample reaches a set amount; outputting the original water sample from the storage cabin, forming a dosing water sample after mixing the original water with a reagent, feeding the dosing water sample into a digestion device, digesting in the digestion device, and cooling; opening a detection light source of a detector, irradiating the dosing water sample by the detection light source through the digestiondevice, reading an optical signal from the detector, and computing the content of the heavy metal; sending data to a computer side by the detector through a wireless signal, and saving the data, thusrealizing real-time online monitoring on the content of the heavy metal in the water. According to the online detecting method disclosed by the invention, 24-hour real-time automatic online detectionon the heavy metal in the water can be realized, and the detection accuracy is high; a detection process is simple and easy to realize, an operator is not required to be on the scene all the time, and labor strength is reduced.

Description

technical field [0001] The invention relates to the technical field of water quality detection methods, in particular to an online detection method for heavy metal content in water quality. Background technique [0002] While the society is developing, it also brings pollution, especially water pollution that seriously affects people's lives. Among them, heavy metals are an important type of pollutant in water. If the content of heavy metals in drinking water exceeds the standard, it will seriously affect people's health. Heavy metals are more common and the content The three most likely to exceed the standard are manganese, copper and iron. in: [0003] 1. Manganese exists in two forms: dissolved and suspended in water. The main sources are domestic sewage and industrial wastewater. Manganese is a trace element needed by life activities, but excessive heavy metal manganese cannot be biodegraded, on the contrary, it can be enriched by hundreds of times under the biomagnif...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): G01N21/78G01N21/31G01N1/44G01N1/38
Inventor 宋健仇建军田芳张晶刘苇陈晓军
Owner 苏州泰坤检测技术有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products