Online detecting method of content of heavy metal in water
A detection method and heavy metal technology, applied in the preparation of test samples, measurement of color/spectral characteristics, material analysis through observation of the influence of chemical indicators, etc., can solve the problems of reducing detection efficiency and achieve improved detection efficiency, Real-time online detection and the effect of reducing work intensity
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Embodiment 1
[0038] Embodiment 1: the heavy metal is copper, and in the S2, the reagent added to the original water sample of the digestion device is a mixed solution of sulfuric acid and nitric acid; heated together until the temperature reaches 120°C, and digested in an acidic environment for 1-10min, Obtain a completely dissolved drug-dosed water sample, adjust the pH to neutral after cooling, add citrate as a masking agent to eliminate interference, add a buffer solution until alkaline, and then add a color developer.
Embodiment 2
[0039] Embodiment 2: Similar in structure to Embodiment 1, the difference is: the heavy metal is iron, and in the S2, the reagent added to the original water sample of the digestion device is hydroxylamine hydrochloride. After the reaction is complete, adjust the pH to 5. Add color developer.
Embodiment 3
[0040] Embodiment 3: Similar to the structure of Embodiment 1, the difference is that: the heavy metal is manganese, and in the S2, the reagent added to the original water sample of the digestion device is a mixed solution of mercuric sulfate-phosphoric acid, and it is combined Heat until the temperature reaches 60°C-70°C, digest in an acidic environment for 1min, and after cooling, a completely dissolved drug-dosed water sample is obtained.
[0041] Compared with the prior art, the beneficial effects of the online detection method of the present invention are mainly reflected in: the automatic control operation of heavy metal content detection is realized, which is convenient for rapid sampling detection; and online detection can be performed in real time to realize wireless transmission and control of detection data, Improve work efficiency and reduce work intensity.
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