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High-temperature lithium-based lubricating grease and preparation method thereof

A lithium-based lubricating grease, high-performance technology, applied in the field of lubricants, can solve problems such as unqualified formulations, reduce energy consumption and equipment wear, excellent anti-oxidation, anti-rust and anti-corrosion properties, and good anti-friction performance Effect

Inactive Publication Date: 2018-03-06
安徽中天石化股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, there are many kinds of lithium-based grease formulas on the market, each with its own strengths and weaknesses, but there are very few products that can take into account all aspects of performance. The main reason is that the formula is unqualified. Therefore, a scientific and reasonable formula is urgently needed in the market Production of high-performance lithium-based greases

Method used

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  • High-temperature lithium-based lubricating grease and preparation method thereof
  • High-temperature lithium-based lubricating grease and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] A kind of high-performance lithium base lubricating grease, comprises the raw material of following weight portion:

[0031] Mineral base oil 80 parts

[0032] 3 parts lithium stearate

[0033] 7 parts lithium lauryl hydroxystearate

[0034] 0.25 parts of zinc dialkyldithiophosphate

[0035] 0.25 parts of antimony dialkyldithiocarbamate

[0036] 0.2 parts of expanded graphite

[0037] Nano copper powder 0.2 parts

[0038] Nano calcium carbonate 0.2 parts

[0039] Nano molybdenum disulfide 0.4 parts

[0040] 0.08 parts of diisooctyl diphenylamine

[0041] 2-naphthol composition 0.12 parts

[0042] 0.1 part of barium dinonylnaphthalenesulfonate

[0043] Benzotriazole 0.1 parts

[0044] 0.2 part of alkyl thiophosphate

[0045] 0.2 parts of chlorobromoalkyl phosphate

[0046] 1 part naphthenic acid.

[0047] The preparation method of above-mentioned high-performance lithium base lubricating grease, comprises the steps:

[0048] Add lithium stearate, lithium la...

Embodiment 2

[0050] A kind of high-performance lithium base lubricating grease, comprises the raw material of following weight portion:

[0051] Mineral base oil 90 parts

[0052] 4 parts lithium stearate

[0053] Lithium lauryl hydroxystearate 10 parts

[0054] 0.5 parts of zinc dialkyldithiophosphate

[0055] 0.5 parts of antimony dialkyldithiocarbamate

[0056] 0.4 parts of expanded graphite

[0057] 0.4 parts of nano copper powder

[0058] Nano calcium carbonate 0.4 parts

[0059] Nano molybdenum disulfide 0.8 parts

[0060] 0.2 parts of diisooctyl diphenylamine

[0061] 0.3 parts of 2-naphthol

[0062] 0.2 parts of barium dinonylnaphthalenesulfonate

[0063] Benzotriazole 0.2 parts

[0064] 0.5 part of alkyl thiophosphate

[0065] Chlorobromoalkyl Phosphate 0.5 parts

[0066] 1.5 parts of naphthenic acid.

[0067] The preparation method of above-mentioned high-performance lithium base lubricating grease, comprises the steps:

[0068] Add lithium stearate, lithium lauryl ...

Embodiment 3

[0070] A kind of high-performance lithium base lubricating grease, comprises the raw material of following weight portion:

[0071] Mineral base oil 100 parts

[0072] Lithium stearate 5 parts

[0073] Lithium lauryl hydroxystearate 15 parts

[0074] 1 part zinc dialkyldithiophosphate

[0075] 1 part antimony dialkyldithiocarbamate

[0076] 0.6 parts of expanded graphite

[0077] 0.6 parts of nano copper powder

[0078] Nano calcium carbonate 0.6 part

[0079] Nano molybdenum disulfide 1.2 parts

[0080] 0.32 parts of diisooctyl diphenylamine

[0081] 0.48 parts of 2-naphthol

[0082] 0.5 parts of barium dinonylnaphthalenesulfonate

[0083] Benzotriazole 0.5 parts

[0084] Alkylthiophosphate 0.8 parts

[0085] Chlorobromoalkyl Phosphate 0.8 parts

[0086] 2 parts naphthenic acid.

[0087] The preparation method of above-mentioned high-performance lithium base lubricating grease, comprises the steps:

[0088] Add lithium stearate, lithium lauryl hydroxystearate, a...

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Abstract

The invention relates to high-temperature lithium-based lubricating grease. The high-temperature lithium-based lubricating grease is prepared from the following raw materials in parts by weight: 80 to100 parts of mineral base oil, 3 to 5 parts of lithium stearate, 7 to 15 parts of lithium 12-hydroxystearate, 0.5 to 2 parts of an extreme pressure anti-wear additive, 1 to 3 parts of a solid additive, 0.2 to 0.8 part of an antioxidant, 0.1 to 0.5 part of an anti-rust agent, 0.1 to 0.5 part of an anti-corrosion agent, 0.2 to 0.8 part of an oily agent, 0.2 to 0.8 part of a flame retardant and 1 to2 parts of a stabilizer. The lithium-based lubricating grease provided by the invention has excellent comprehensive performance; the stabilizer is added so that the structure stability of the lubricating grease is improved, and properties including the colloid stability, the mechanical stability, the water resistance and the like of the lubricating grease are greatly improved; the extreme pressure anti-wear additive and the solid additive, which have a mutual synergistic effect, are added so that the lubricating grease has relatively good friction reduction performance and anti-wear performance and relatively good stability; the energy consumption of equipment in an operation process and abrasion on the equipment are easy to reduce and the service life of the equipment is prolonged. Meanwhile, the high-temperature lithium-based lubricating grease has good anti-oxidization performance and anti-rust and anti-corrosion performance.

Description

technical field [0001] The invention belongs to the field of lubricants, in particular to a high-performance lithium-based lubricating grease and a preparation method thereof. Background technique [0002] Grease is a lubricating material between liquid and solid, and its output accounts for far less than lubricating oil in the entire lubricating product. However, the lubricating performance of grease is better than that of lubricating oil. At normal temperature, it can be adsorbed on the metal surface without flowing; when heated or mechanically affected, the grease becomes thinner and can lubricate the friction surface like a liquid. When heated When the action and mechanical action gradually diminish to disappear, the grease returns to its state. Because of this particularity, lubricating grease has been widely used in the fields of industry, agriculture, transportation, defense industry, etc., and has become one of the most promising lubricating materials. [0003] Lit...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M169/06C10N30/06C10N30/10C10N30/12
CPCC10M169/06C10M2201/041C10M2201/05C10M2201/062C10M2201/066C10M2203/1006C10M2207/025C10M2207/1265C10M2207/1285C10M2207/16C10M2215/064C10M2215/223C10M2219/044C10M2219/068C10M2223/04C10M2223/045C10N2030/06C10N2030/10C10N2030/12C10N2030/26C10N2010/10C10N2010/02C10N2010/04
Inventor 高晓谋高荣权何甲生
Owner 安徽中天石化股份有限公司
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