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A kind of preparation method of superfine denier polyester fdy yarn for high-density fabric

A technology of ultra-fine denier polyester and fabric, applied in the field of polyester spinning, can solve the problems affecting the continuity and safety of the production process, the rapid rise of filter pressure difference, and the reduction of filter service life, so as to ensure the spinnability Sex, reduce impurities, reduce the effect of pressure rise

Active Publication Date: 2020-10-02
JIANGSU HENGKE ADVANCED MATERIALS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] However, due to the addition of the third component in the CDP melt, its apparent viscosity is relatively large, and the impurities produced in the production process also increase accordingly, causing the pressure of some spinning components and the pressure difference of the filter to rise faster. There are carbonized cokes on the inner wall of the pipeline. These carbonized cokes adhere to the inner wall of the pipeline, which is easy to cause blockage of the pipeline system and is not easy to be removed, which brings great difficulties to the dredging of the pipeline. In addition, in the production of this kind of fiber In the process, the service life of the filter is greatly reduced, generally only one week, while the service life of some other spinning components is generally only 10 days, so frequent cleaning and replacement of the spinning components are required, which will not only increase the operating cost, but also Will affect the continuity and safety of the entire production process

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0050] A kind of preparation method of superfine denier polyester FDY silk for high-density fabric, the steps are as follows:

[0051] a) preparing a spinning melt;

[0052] (1) transesterification reaction prepares bishydroxyethyl isophthalate-5-sodium sulfonate;

[0053] First, dimethyl isophthalate-5-sodium benzenesulfonate and ethylene glycol with a molar ratio of 10:1 are put into the preparation kettle, and the catalyst Zn(Ac) is added. 2 Carry out the transesterification reaction at 175 ℃ and end when the distillation amount of water reaches 90% of the theoretical value, obtain bishydroxyethyl isophthalate-5-sodium sulfonate, then add ethylene glycol, sodium ethylene glycol and Sulfuric acid is modulated to obtain the ethylene glycol solution containing 30wt% bishydroxyethyl isophthalate-5-sodium sulfonate, wherein catalyst Zn(Ac) 2 The addition of dimethyl isophthalate-5-sodium benzene sulfonate is 0.2wt% of the addition of dimethyl isophthalate-5-sodium benzene sulf...

Embodiment 2

[0073] A kind of preparation method of superfine denier polyester FDY silk for high-density fabric, the steps are as follows:

[0074] a) preparing a spinning melt;

[0075] (1) transesterification reaction prepares bishydroxyethyl isophthalate-5-sodium sulfonate;

[0076] First, put dimethyl isophthalate-5-sodium benzenesulfonate and ethylene glycol into the preparation kettle with a molar ratio of 11:1, add the catalyst Zn(Ac) 2 Carry out the transesterification reaction at 178°C with the anti-ether agent NaAc until the distilled amount of water reaches 92% of the theoretical value to obtain bishydroxyethyl isophthalate-5-sodium sulfonate, and then add ethylene glycol , sodium ethylene glycol and sulfuric acid are modulated to obtain the ethylene glycol solution containing 31wt% bishydroxyethyl isophthalate-5-sodium sulfonate, wherein the catalyst Zn(Ac) 2 The addition amount is 0.3wt% of the addition amount of dimethyl isophthalate-5-sodium benzenesulfonate, the addition ...

Embodiment 3

[0094] A kind of preparation method of superfine denier polyester FDY silk for high-density fabric, the steps are as follows:

[0095] a) preparing a spinning melt;

[0096] (1) transesterification reaction prepares bishydroxyethyl isophthalate-5-sodium sulfonate;

[0097] First, put dimethyl isophthalate-5-sodium benzenesulfonate and ethylene glycol into the preparation kettle with a molar ratio of 12:1, and add the catalyst Zn(Ac) 2 Carry out the transesterification reaction at 179°C with the anti-ether agent NaAc until the distilled amount of water reaches 91% of the theoretical value to obtain bishydroxyethyl isophthalate-5-sodium sulfonate, and then add ethylene glycol , sodium ethylene glycol and sulfuric acid are modulated to obtain the ethylene glycol solution containing 32wt% bishydroxyethyl isophthalate-5-sodium sulfonate, wherein the catalyst Zn(Ac) 2 The addition amount is 0.25wt% of the addition amount of dimethyl isophthalate-5-sodium benzene sulfonate, the add...

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Abstract

The invention relates to a preparation method of superfine polyester FDY yarns for high density fabric. The preparation method comprises the following steps: firstly mixing dimethyl isophthalate-5-sodium benzenesulfonate, glycol and a catalyst, then performing ester interchange reaction, adding glycol, sodium glycol and sulfuric acid to be blended after reaction, mixing terephthalic acid, glycol,a catalyst and a stabilizer and performing esterification reaction, adding a product formed by blending after ester exchange reaction into a reaction system reaching an esterification reaction end point to be subjected to polycondensation reaction, so as to obtain spinning melt, and finally performing measuring, extruding, cooling, oil applying, stretching, heat setting and coiling on the spinningmelt, so as to obtain the superfine polyester FDY yarn for high density fabric. The method reduces impurities produced during the production of the polyester FDY yarns, thereby reducing the pressurerise of spinning components and a filter, prolongs the service cycle, guarantees the continuity and the safety of the whole production process, and has a good economic value and a popularization value.

Description

technical field [0001] The invention belongs to the field of polyester spinning, and relates to a method for preparing superfine denier polyester FDY yarns for high-density fabrics. Background technique [0002] High-density fabric refers to a type of fabric whose warp and weft yarn raw material yarn number is low and its warp and weft density is large. Fabric density can be divided into warp density and weft density. Generally, the finer the yarn count, the greater the possible density. Therefore, high-density fabrics are often based on the premise of high count. Permeable, belonging to the category of high-end fabrics. When dividing and defining fabrics according to the actual production of chemical fiber filament fabrics and their uses, it is customary to identify fabrics with a denier below 50D (55.5dtex) and a warp and weft density of 1200 threads / 10cm and above as high-count (low denier) and high-density fabrics. fabric. [0003] Polyester is generally used as a raw...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01F6/92D01F1/10C08G63/688C08G63/86
Inventor 王永锋印成王峰张正勇
Owner JIANGSU HENGKE ADVANCED MATERIALS CO LTD
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