Graphene and silver nanowire loaded silk/sodium alginate porous composite material
A technology of porous composite material and silver nanowire, which is applied in the field of nanocomposite materials and achieves the effect of huge application value
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Embodiment 1
[0020] (1) Disperse sodium alginate in deionized water at room temperature, bath ratio 1:50, slowly add 1g / L polyamide-amine PAMAM aqueous solution, wherein the volume ratio of PAMAM aqueous solution to sodium alginate aqueous solution is 1:1, After reacting for 24 hours, it was repeatedly washed with distilled water and ethanol, and dried to obtain PAMAM-modified sodium alginate. (2) Dissolve silk protein in deionized water to prepare a 1g / L aqueous solution. Slowly drop 1g / L ferric chloride aqueous solution into the silk protein aqueous solution at 50°C and stir evenly. The mass ratio of protein to ferric chloride is 1:1, after stirring at a constant speed at 60°C for 1 hour, slowly add the PAMAM modified sodium alginate in step 1, the mass ratio of the modified sodium alginate to silk protein is 1:1 , after ultrasonically mixing evenly, pour it into the mold, put it in liquid nitrogen for 1min, take it out and put it in a -20°C refrigerator for 6h, freeze it in a Thermo ult...
Embodiment 2
[0022] (1) Disperse sodium alginate in deionized water at room temperature, bath ratio 1:50, slowly add 10g / L polyamide-amine PAMAM aqueous solution, wherein the volume ratio of PAMAM aqueous solution to sodium alginate aqueous solution is 1:5, After reacting for 24 hours, it was repeatedly washed with distilled water and ethanol, and dried to obtain PAMAM-modified sodium alginate. (2) Dissolve silk protein in deionized water to prepare a 10g / L aqueous solution, slowly drop 10g / L ferric sulfate aqueous solution into the silk protein aqueous solution at 70°C, and stir evenly, wherein the silk protein The mass ratio to ferric sulfate is 5:1, after stirring at a constant speed at 60°C for 1 hour, slowly add the PAMAM modified sodium alginate in step 1, the mass ratio of the modified sodium alginate to silk protein is 1:5, ultrasonic After mixing evenly, pour it into a mold, put it in liquid nitrogen for 1 minute, take it out and put it in a -20°C refrigerator for 6 hours, freeze ...
Embodiment 3
[0024] (1) Disperse sodium alginate in deionized water at room temperature, bath ratio 1:50, slowly add 50g / L polyamide-amine PAMAM aqueous solution, wherein the volume ratio of PAMAM aqueous solution to sodium alginate aqueous solution is 1:10, After reacting for 24 hours, it was repeatedly washed with distilled water and ethanol, and dried to obtain PAMAM-modified sodium alginate. (2) Dissolve silk protein in deionized water to prepare a 50g / L aqueous solution, slowly drop 50g / L ferric nitrate aqueous solution into the silk protein aqueous solution at 80°C, and stir evenly, wherein the silk protein The mass ratio to ferric nitrate is 10:1, after stirring at a constant speed at 60°C for 1 hour, slowly add the PAMAM modified sodium alginate in step 1, the mass ratio of the modified sodium alginate to silk protein is 1:10, ultrasonic After mixing evenly, pour it into a mold, put it in liquid nitrogen for 1 minute, take it out and put it in a -20°C refrigerator for 6 hours, free...
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