A kind of Dazhu Hongjingtian capsule fingerprint and its construction method
A fingerprint, Rhodiola technology, used in instruments, measuring devices, scientific instruments, etc.
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[0037] 1 material
[0038] 1.1 Instrument
[0039] Agilent 1100 high-performance liquid chromatography, Agilent 1290-6538 ultra-high performance liquid chromatography-mass spectrometry (Agilent Technologies, Germany); ST-16R high-speed refrigerated centrifuge (Thermo Fisher Scientific Co., Ltd.); AL104 type One-ten-thousandth balance, MettlerXS205 one-hundred-thousandth balance (Mettler-Toledo Shanghai Instrument Co., Ltd.); KH2200B ultrasonic cleaner (Kunshan Hechuang Ultrasonic Instrument Co., Ltd.); HSC-24A nitrogen blowing instrument ( Tianjin Hengao Technology Development Co., Ltd.); Mill-Q pure water system (Millipore, USA)
[0040] 1.2 Reagents
[0041] Methanol (chromatographically pure, Merck, USA), acetonitrile (chromatographically pure, Merck, USA), formic acid (Merck, Germany), and other reagents were of analytical grade, purchased from Nanjing Chemical Reagent Co., Ltd.; ultrapure water.
[0042] 1.3 Reference substance
[0043] Reference substances gallic aci...
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