Core-shell structure Si/C material, preparation method and application
A core-shell structure, suspension technology, applied in structural parts, electrical components, battery electrodes, etc., can solve the problems of long synthesis process, complex preparation method, difficult material performance, etc., achieve excellent electrochemical performance, simplify Preparation process, the effect of promoting decomposition
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[0038] figure 1 It is a schematic diagram of the Si / C material preparation method of the core-shell structure Si / C material of the present invention. As shown in the figure, the preparation method of the core-shell structure Si / C material of the present invention specifically includes the following steps:
[0039] (1) Prepared Fe(NO 3 ) 3 Dissolved in deionized water to obtain Fe(NO 3 ) 3 solution, and take Si powder for use, wherein the Si powder is nano Si powder or micron Si powder, and the mass ratio range of Fe and Si is 5:1~1:1;
[0040] (2) Put the weighed Si powder into Fe(NO 3 ) 3 solution, and add a dispersant, and ultrasonically stir the Si powder to disperse evenly to form a suspension. The dispersant includes a non-polar liquid, preferably absolute ethanol;
[0041] (3) Pour the suspension obtained in step (2) into a low-temperature resistant container, and pour clean liquid nitrogen into the suspension to freeze to form ice-state Si / Fe(NO 3 ) 3 , preferab...
Embodiment 1
[0052] Take by weighing the nano-Si powder of 100mg for subsequent use, take by weighing an appropriate amount of Fe(NO 3 ) 3Dissolve in 20mL deionized water; put the weighed nano-Si powder into Fe(NO 3 ) 3 solution, and Fe:Si=3:1 (mass ratio), add 3mL of absolute ethanol to help the dispersion of nano-Si powder, ultrasonically stir and disperse evenly to form a suspension; pour the above suspension into a plastic container, pour Clean liquid nitrogen is frozen to form ice Si / Fe(NO 3 ) 3 ; the above ice Si / Fe (NO 3 ) 3 Put it into the pre-cooled freeze dryer for freeze-drying, turn on the vacuum pump, the temperature of the cold well of the freeze dryer is -70°C, the vacuum degree is 1Pa, and the freeze-drying time is 48h; take out the above-mentioned freeze-dried samples and put them into a tube furnace, N 2 Warm up to 400°C under atmosphere, N 2 Change the atmosphere to C 2 h 2 Change back to N after the atmosphere is kept warm for 40 minutes 2 , cooled to room te...
Embodiment 2
[0054] Take by weighing the nano-Si powder of 100mg for subsequent use, take by weighing an appropriate amount of Fe(NO 3 ) 3 Dissolve in 20mL deionized water; put the weighed nano-Si powder into Fe(NO 3 ) 3 solution, and Fe:Si=3:1 (mass ratio), add 3mL of absolute ethanol to help the dispersion of nano-Si powder, ultrasonically stir and disperse evenly to form a suspension; pour the above suspension into a plastic container, pour Clean liquid nitrogen is frozen to form ice Si / Fe(NO 3 ) 3 ; the above ice Si / Fe (NO 3 ) 3 Put it into the pre-cooled freeze dryer for freeze-drying, turn on the vacuum pump, the temperature of the cold well of the freeze dryer is -70°C, the vacuum degree is 1Pa, and the freeze-drying time is 48h; take out the above-mentioned freeze-dried samples and put them into a tube furnace, N 2 Warm up to 500°C under atmosphere, N 2 Change the atmosphere to C 2 h 2 Change back to N after the atmosphere is kept warm for 40 minutes 2 , cooled to room t...
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