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Deep eutectic solvent and method for extracting anthraquinone from radix et rhizoma rhei by using deep eutectic solvent

A technology of deep eutectic solvent and extraction method, which is applied in organic chemical methods, chemical instruments and methods, quinone separation/purification, etc., to achieve the effects of improving extraction rate, reducing environmental pollution, and shortening extraction time

Active Publication Date: 2017-09-29
SICHUAN AGRI UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

But no one has used DESs for the extraction of rhubarb anthraquinones

Method used

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  • Deep eutectic solvent and method for extracting anthraquinone from radix et rhizoma rhei by using deep eutectic solvent
  • Deep eutectic solvent and method for extracting anthraquinone from radix et rhizoma rhei by using deep eutectic solvent
  • Deep eutectic solvent and method for extracting anthraquinone from radix et rhizoma rhei by using deep eutectic solvent

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Embodiment 1

[0024] Embodiment 1 The method for extracting anthraquinone in rhubarb by deep eutectic solvent of the present invention

[0025] 1. Materials and Reagents

[0026] Rhubarb powder; macroporous adsorption resin DM130; absolute ethanol, concentrated sulfuric acid (excellent grade), lactic acid, glucose, phosphoric acid, methanol (chromatographically pure, Fisher), aloe-emodin, emodin, rhein, chrysophanol, emodin Standard methyl ether (content ≥98%, Chengdu Zhibiao Huachun Biotechnology Co., Ltd.), all of which are analytically pure unless otherwise indicated.

[0027] 2. Experimental equipment

[0028] LC-20A high performance liquid chromatograph (Shimadzu, Japan), KQ-300GDV constant temperature numerical control ultrasonic cleaner, BT 124s electronic balance, LGJ-12 freeze dryer, WP-Z-UV laboratory ultrapure water machine , FW135 Chinese herbal medicine grinder, 80-1 electric centrifuge, DF-101S collector type constant temperature heating magnetic stirrer.

[0029] 3. Experi...

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Abstract

The invention provides a deep eutectic solvent which is composed of lactic acid, D-(+)-glucose and water, wherein the mole ratio of the lactic acid to the D-(+)-glucose in the deep eutectic solvent is (1-2):(1-5), and the water content is 0-80% (V / V). The invention also provides application of the deep eutectic solvent and a method for extracting anthraquinone from radix et rhizoma rhei by using the deep eutectic solvent. When being used for extracting anthraquinone from radix et rhizoma rhei, the deep eutectic solvent replaces chloroform and other toxic organic solvents in the traditional extraction, reduces the environmental pollution of the radix et rhizoma rhei industry, and thus, is green and environmentally friendly. The deep eutectic solvent has high extraction efficiency and is recyclable and reusable, thereby greatly lowering the extraction cost, and providing a new technical means for reasonable development and utilization of radix et rhizoma rhei resources.

Description

technical field [0001] The invention provides a deep eutectic solvent and a method for extracting anthraquinone in rhubarb, belonging to the field of comprehensive utilization of Chinese medicinal material resources. Background technique [0002] Rhubarb is a herbal medicine included in the Pharmacopoeia of the People's Republic of China (2015 Edition, Part One), and its medicinal sources are Rheum palmatum L., Rheumtanguticum Maxim.exBalf. or Rheum officinaleBaill The dried roots and rhizomes of . Bitter in taste, cold in nature, it returns to the spleen, stomach, liver, large intestine, and heart meridian. It has the functions of purging stagnation, clearing away heat and fire, cooling blood and detoxifying, removing blood stasis and dredging menstrual flow. The main active ingredients are rhein, emodin, and chrysophanol , emodin methyl ether, aloe-emodin, etc. Modern pharmacological studies have shown that rhubarb has the functions of purging, antibacterial, anti-tumor,...

Claims

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Application Information

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IPC IPC(8): C07B63/00C07C51/42C07C51/47C07C66/02C07C46/10C07C50/34
CPCC07B63/00C07C46/10C07C51/42C07C51/47C07C50/34C07C66/02
Inventor 张利吴一超李亚波吴鹏姜媛媛魏良益刘天池
Owner SICHUAN AGRI UNIV
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