Application of Tibetan capillaris in preparing a medicine for treating viral hepatitis B
A viral hepatitis and drug technology, applied in the direction of antiviral agents, drug combinations, pharmaceutical formulas, etc., can solve the problems of inability to completely remove hepatitis B virus accurately and effectively
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experiment example 1
[0014] Experimental example 1 Selection of extraction solvent and rough selection of extraction method
[0015] Get the coarse powder 80 grams of Chinese herbal medicine, test according to the scheme in table 1, test result is as shown in table 2:
[0016] Table 1 Different extraction schemes
[0017] Option One Decoct and extract twice, each time for 2 hours, the amount of water added is 10 times the amount of medicinal materials each time Option II Reflux extraction 2 times, 2 hours each time, add 5% ethanol to 10 times the amount of medicinal materials third solution Reflux extraction 2 times, 2 hours each time, add 40% ethanol to 10 times the amount of medicinal materials Option four Reflux extraction 2 times, 2 hours each time, add 80% ethanol to 10 times the amount of medicinal materials Option five Reflux extraction 2 times, 2 hours each time, add 95% ethanol to 10 times the amount of medicinal materials Option six Optio...
experiment example 2
[0021] Experimental example 2 Investigation on water extraction process of Chinese herbal medicines
[0022] 1. The influence of the processing length of medicinal materials on the paste yield
[0023] Weigh 80g of Chinese medicinal materials, soak the medicinal materials with 10 times the amount of water for 30 minutes, decoct 2 times for 2 hours each time, filter, combine the filtrates, concentrate, and measure the cream yield. The results are shown in Table 3:
[0024] Table 3 Effect of processing length of medicinal materials on ointment yield
[0025]
[0026] It can be seen from the above table 3 that the ointment yield of the coarse powder of medicinal materials is the highest, but because the medicinal liquid is difficult to filter after the coarse powder of medicinal materials is extracted, although the medicinal residues can be squeezed out mechanically during the experiment, it is not suitable for large-scale industrial production; and The extracting rate of med...
experiment example 3
[0043] Experimental Example 3 Extraction Scheme Verification
[0044] According to the optimized test conditions, weigh 10000g of Chinese herbal medicine processed into 1.0cm section, extract twice, add 8 times the amount of water to soak for 30 minutes, decoct for 2 hours, and add 8 times the amount of water to decoct for the second time After 2 hours of extraction, the extract was filtered, the filtrate was concentrated, and dried under reduced pressure (at a temperature of 65-75°C and a vacuum of 0.08-0.1Mpa) to measure the yield of the paste. The results are shown in Table 8:
[0045] Table 8 Extraction scheme verification
[0046]
[0047] It can be seen from the above table 8 that it is reasonable and feasible to use the optimized test conditions to extract Chinese herbal medicines.
[0048] The specific method for the determination of the cream yield described in the above experimental example is: take the clear cream concentrated to a relative density of 1.20-1.30 (m...
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