Preparation method of long-preservation-time water-washable fruit wax
A technology of water washing and fruit wax, which is applied in the direction of protecting fruits/vegetables with a coating protective layer, which can solve the problems of accelerating the accumulation of volatile odorous substances, strengthening anaerobic respiration of fruits, and difficult cleaning, achieving good water retention and easy cleaning. Water cleaning, the effect of wide application prospects
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example 1
[0017] Add 120g of methyl hydrogen-containing silicone oil, 100g of octadecatrienoic acid, 10g of allyl polyoxyethylene ether and 80g of isopropanol to a three-necked flask equipped with a thermometer, a stirrer and a condenser, and put the three-necked flask into In a water bath, feed nitrogen gas into the flask at a rate of 10mL / min, and at the same time raise the temperature to 75°C at a rate of 5°C / min, then add 1mL of 5% hydrochloric acid solution dropwise, and control it within 5min After completion of the dropwise addition, heat-retain and stir for 2 hours. After the reaction, distill under reduced pressure for 15 minutes to obtain a transparent liquid for later use; weigh 3g of fatty alcohol polyoxyethylene ether, 4g of cocamide methyl and 3g of lauramide respectively. Mix propyl betaine to obtain a mixed emulsifier, then weigh 15g of oleic acid, 10g of palm wax and 5g of abietic acid and add them to 30mL of deionized water, stir and mix for 20min, then add 200mL of dei...
example 2
[0020]Add 130g of methyl hydrogen silicone oil, 110g of octadecatrienoic acid, 15g of allyl polyoxyethylene ether and 100g of isopropanol in sequence to a three-necked flask equipped with a thermometer, a stirrer and a condenser, and put the three-necked flask into In a water bath, feed nitrogen gas into the flask at a rate of 15mL / min, and at the same time raise the temperature to 80°C at a rate of 7°C / min, then add 2mL of 5% hydrochloric acid solution dropwise, and control it within 8min After completion of the dropwise addition, heat preservation and stirring for 2.5 hours. After the reaction, distill under reduced pressure for 20 minutes. After the distillation, a transparent liquid is obtained for subsequent use; respectively weigh 4g of fatty alcohol polyoxyethylene ether, 5g of cocamide methyl and 4g of lauryl Mix amidopropyl betaine to obtain a mixed emulsifier, then weigh 17g oleic acid, 15g palm wax and 10g abietic acid and add them to 40mL deionized water, stir and m...
example 3
[0023] Add 150g of methyl hydrogen-containing silicone oil, 120g of octadecatrienoic acid, 20g of allyl polyoxyethylene ether and 120g of isopropanol to a three-necked flask equipped with a thermometer, a stirrer and a condenser, and put the three-necked flask into In a water bath, feed nitrogen into the flask at a rate of 20mL / min, and at the same time raise the temperature to 85°C at a rate of 10°C / min, then add 3mL of 5% hydrochloric acid solution dropwise, and control it within 10min After completion of the dropwise addition, keep warm and stir for 3 hours. After the reaction, distill under reduced pressure for 25 minutes. After the distillation, a transparent liquid is obtained for later use. Weigh 5g of fatty alcohol polyoxyethylene ether, 6g of cocamide methyl and 5g of laurylamide respectively. Mix propyl betaine to obtain a mixed emulsifier, then weigh 20g of oleic acid, 20g of palm wax and 15g of abietic acid and add them to 50mL of deionized water, stir and mix for 3...
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