Method for preparing silver-loaded chitosan medical dressing
A technology of chitosan and silver nitrate, which is applied in medical science, absorbent pads, textiles and papermaking, etc., can solve the problems of chemical reducing agents affecting application, low efficiency and high production cost, and achieve excellent broad-spectrum antibacterial properties and simple treatment methods , fixed effect
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Embodiment 1
[0027] Utilize loquat leaf to prepare nano-silver aqueous solution, comprises the following steps:
[0028] (1) Take by weighing 5g of dried and pulverized loquat leaf powder in a 250mL Erlenmeyer flask, add 150mL of deionized water and mix uniformly, leaching for 90min at a temperature of 80°C, then filter and centrifuge to remove the loquat leaf powder residue, Obtain loquat leaf extract;
[0029] (2) Add 2 mL of loquat leaf extract to 50 mL of 1 mmol / L silver nitrate solution, mix well, adjust the pH value to 6, and react at 80° C. for 60 min to obtain a nano-silver aqueous solution.
[0030] The ultraviolet-visible absorption spectrum of the nano-silver that the present embodiment makes is as attached figure 1 shown by figure 1 It can be seen that a typical nano-silver absorption peak has occurred at 435nm, which proves that nano-silver particles have been generated in the aqueous solution; figure 2 as shown, figure 2 It shows that the nano-silver prepared from loqua...
Embodiment 2
[0036] Utilize loquat nucleus to prepare nano-silver, comprises the following steps:
[0037] (1) Take by weighing 5g of dried and pulverized loquat core powder in a 250ml Erlenmeyer flask, add 100mL of deionized water therein, mix well and then leaching for 90min at a temperature of 90°C, then filter and centrifuge to remove the loquat core powder residue, Obtain loquat core extract.
[0038] (2) Add 5 mL of loquat core extract to 50 mL of 1 mmol / L silver nitrate solution, mix well, adjust the pH value to 8-9, and then place it at 60° C. for 60 min to obtain a nano silver aqueous solution.
[0039] Utilize the nano-silver aqueous solution prepared by the present embodiment to prepare silver-loaded chitosan medical dressing, comprising the following steps:
[0040] (1) First use 0.1mol / L acetic acid solution to pre-adjust the pH value of the nano-silver aqueous solution prepared in this example to 5.6, then immerse 1g of chitosan fiber non-woven fabric in it according to the ba...
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