A kind of p-type lamsno amorphous oxide semiconductor film and preparation method thereof
A technology of amorphous oxide and semiconductor, which is applied in the manufacture of semiconductor/solid-state devices, semiconductor devices, transistors, etc., to achieve the effect of simple preparation process, low cost and promotion of development
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Embodiment 1
[0025] (1) with high purity La 2 o 3 , Nb 2 o 5 and SnO 2 Powder as raw material, mixed, ground, at 1100°C O 2 Sintering under the atmosphere to make LaNbSnO ceramic sheet as the target material, in which the atomic ratio of La, Nb and Sn is 1:1:0.1;
[0026] (2) Using the radio frequency magnetron sputtering method, install the substrate and target in the sputtering reaction chamber, and evacuate to a vacuum degree of 1×10 -3 Pa;
[0027] (3) Passing Ar-O 2 For the working gas, the gas pressure is 9Pa, Ar-O 2 The flow volume ratio is 10:5, the sputtering power is 140W, and the substrate temperature is 500°C. 2 Under the bombardment of ions, the atoms and molecules on the surface of the target are sputtered out, and a thin film is deposited on the substrate. 2 Naturally cooled to room temperature under atmosphere to obtain p-type LaNbSn 0.1 o 4.2 Amorphous thin film.
[0028] Using quartz as the substrate, p-type LaNbSn was prepared according to the above growth st...
Embodiment 2
[0030] (1) with high purity La 2 o 3 , Nb 2 o 5 and SnO 2 Powder as raw material, mixed, ground, at 1100°C O 2 Sintering under the atmosphere to make LaNbSnO ceramic sheet as the target material, in which the atomic ratio of La, Nb and Sn is 1:1:0.25;
[0031] (2) Using the radio frequency magnetron sputtering method, install the substrate and target in the sputtering reaction chamber, and evacuate to a vacuum degree of 1×10 -3 Pa;
[0032] (3) Passing Ar-O 2 For the working gas, the gas pressure is 10Pa, Ar-O 2The flow volume ratio is 10:6, the sputtering power is 150W, and the substrate temperature is 350°C. 2 Under the bombardment of ions, the atoms and molecules on the surface of the target are sputtered out, and a thin film is deposited on the substrate. 2 Naturally cooled to room temperature under atmosphere to obtain p-type LaNbSn 0.25 o 4.5 Amorphous thin film.
[0033] Using quartz as the substrate, p-type LaNbSn was prepared according to the above growth ...
Embodiment 3
[0035] (1) with high purity La 2 o 3 , Nb 2 o 5 and SnO 2 Powder as raw material, mixed, ground, at 1100°C O 2 Sintering under the atmosphere to make LaNbSnO ceramic sheet as the target material, in which the atomic ratio of La, Nb and Sn is 1:1:0.4;
[0036] (2) Using the radio frequency magnetron sputtering method, install the substrate and target in the sputtering reaction chamber, and evacuate to a vacuum degree of 1×10 -3 Pa;
[0037] (3) Passing Ar-O 2 For the working gas, the gas pressure is 12Pa, Ar-O 2 The flow volume ratio is 10:7, the sputtering power is 150W, and the substrate temperature is 200°C. 2 Under the bombardment of ions, the atoms and molecules on the surface of the target are sputtered out, and a thin film is deposited on the substrate. 2 Naturally cooled to room temperature under atmosphere to obtain p-type LaNbSn 0.4 o 4.8 Amorphous thin film.
[0038] Using quartz as the substrate, p-type LaNbSn was prepared according to the above growth s...
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