Amorphous compound magnetic core and preparation method thereof
A technology of amorphous alloy and magnetic core, which is applied in the field of amorphous composite magnetic core and its preparation, can solve the problems of low transient impedance, easy damage of switching devices, low magnetic permeability, etc., and achieve the solution of transient current distortion, The effect of improving the power factor of the power supply and increasing the initial magnetic permeability
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[0028] The present invention also provides a preparation method of the amorphous composite magnetic core according to the above technical solution, comprising the following steps:
[0029] (1) mixing the magnetic amorphous alloy powder with the insulating coating agent to obtain a mixed material;
[0030] (2) molding the mixture obtained in the step (1) and the ferrite core, so that the mixture is coated on the surface of the ferrite core to obtain a blank;
[0031] (3) preheating the green body obtained in the step (2) to obtain an amorphous composite magnetic core precursor;
[0032] (4) annealing the amorphous composite magnetic core precursor obtained in the step (3) to obtain an amorphous composite magnetic core.
[0033] In the present invention, the magnetic amorphous alloy powder is mixed with an insulating coating agent to obtain a mixed material. In the present invention, the mixing temperature is preferably 15-130°C, more preferably 25-100°C, and most preferably 5...
Embodiment 1
[0044] Mixing 1K101 magnetic amorphous alloy powder with a weight of 150 mesh and a weight of 27.65g, 1g phosphoric acid, 1g sodium silicate and 0.35g kaolin at room temperature for 5min at a change rate of 5-60r / min to obtain a mixture;
[0045] Put 20g of the mixed material into the mold of OD33.02mm×ID19.9mm×HT15mm, then put 3g of nickel-zinc ferrite powder core with the size of OD30mm×ID25mm×HT3mm into the mold, and finally put the remaining 10g of the mixed material into the mold. into the mold, the pressure reaches 21t / cm 2 After holding for 10s, the blank is obtained by unmolding;
[0046] Under the condition of vacuum degree of 0.08Pa, the green body is preheated at 200℃ for 50min to obtain an amorphous composite magnetic core precursor;
[0047] Under the same vacuum conditions, the amorphous composite magnetic core was obtained at a constant temperature of 420° C. for 60 minutes, followed by cooling in the furnace.
Embodiment 2
[0049] Mixing 250 mesh 1K101 magnetic amorphous alloy powder with a weight of 29.56 g, 0.22 g of ethyl orthosilicate and 0.22 g of zinc stearate at a rate of change of 5-60 r / min at 80°C for 10 min to obtain a mixed material;
[0050] Put 20g of the mixed material into a mold of OD33.02mm×ID19.9mm×HT15mm, then put 3g of manganese-zinc ferrite cores with a size of OD30mm×ID25mm×HT3mm into the mold, and finally put the remaining 10g of mixed material into the mold. into the mold, pressurized 18t / cm 2 Hold for 15s, unmold to obtain a green body;
[0051] Preheating at 250°C for 30min in a nitrogen gas flow rate of 5L / min to obtain an amorphous composite magnetic core precursor;
[0052] In the same atmosphere, the amorphous composite magnetic core was obtained by annealing at 390°C for 80min.
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