Aerogel PET (polyethylene terephthalate) master batch and manufacturing technique thereof
A manufacturing process and aerogel technology, applied in the field of aerogel PET masterbatch and its manufacturing process, can solve the problems of poor thermal insulation effect, low toughness, easy fracture, etc., and achieve good wear resistance, high toughness, The effect of excellent thermal insulation
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Embodiment 1
[0024] Embodiment 1 of the present invention provides an airgel PET masterbatch, the airgel PET masterbatch includes toluene diisocyanate, polyvinylpyrrolidone, airgel, PET chips, the toluene diisocyanate, polyvinylpyrrolidone, airgel The mass ratio of gel and PET slices is 0.01:0.01:5:75. Wherein, the particle size of the airgel is 50, and the PET slice viscosity is greater than 0.85 dI / g.
[0025] The manufacturing process of above-mentioned airgel PET masterbatch comprises the following steps:
[0026] 1) Prepare materials according to the following mass ratio: the mass ratio of the toluene diisocyanate, polyvinylpyrrolidone, aerogel, and PET chips is 0.01:0.01:5:75;
[0027] 2) Mix toluene diisocyanate, polyvinylpyrrolidone and aerogel evenly, and perform activation treatment for 1 hour to obtain the mixed material A;
[0028] 3) Add PET slices to the mixture A, mix evenly, and dry at 120°C for 6 hours to obtain the mixture B;
[0029] 4) Put the dried mixed material B ...
Embodiment 2
[0033] Embodiment 1 of the present invention provides an airgel PET masterbatch, the airgel PET masterbatch includes hexamethylene diisocyanate, polydimethylsilicone oil, aerogel, PET chips, and the hexamethylene The mass ratio of diisocyanate, polydimethylsiloxane, aerogel, and PET chips is 0.01:0.01:5:150. Wherein, the particle size of the airgel is 200nm, and the PET slice viscosity is greater than 0.85dI / g.
[0034] The manufacturing process of above-mentioned airgel PET masterbatch comprises the following steps:
[0035] 1) Prepare materials according to the following mass ratio: the mass ratio of the hexamethylene diisocyanate, polydimethylsilicone, aerogel, and PET chips is 0.01:0.01:5:150;
[0036] 2) Mix hexamethylene diisocyanate, polydimethyl silicone oil and airgel evenly, and perform activation treatment for 1 hour to obtain the mixed material A;
[0037] 3) Add PET slices to the mixture A, mix evenly, and dry at 120°C for 6 hours to obtain the mixture B;
[00...
Embodiment 3
[0042] Embodiment 1 of the present invention provides a kind of airgel PET masterbatch, and described airgel PET masterbatch comprises triphenylmethane triisocyanate, polyvinylpyrrolidone, aerogel, PET chips, and described triphenylmethane triisocyanate, polyvinylpyrrolidone The mass ratio of vinylpyrrolidone, airgel, and PET slices is 0.01:0.01:5:75-150. Wherein, the particle size of the airgel is 50-200nm, and the PET slice viscosity is greater than 0.85dI / g.
[0043] The manufacturing process of above-mentioned airgel PET masterbatch comprises the following steps:
[0044] 1) Prepare materials according to the following mass ratio: the mass ratio of triphenylmethane triisocyanate, polyvinylpyrrolidone, aerogel, and PET chips is 0.01:0.01:5:100;
[0045] 2) Mix triphenylmethane triisocyanate, polyvinylpyrrolidone and aerogel evenly, and perform activation treatment for 1 hour to obtain the mixed material A;
[0046] 3) Add PET slices to the mixture A, mix evenly, and dry a...
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