Power type nickel-zinc ferrite material and preparation method thereof
A nickel-zinc ferrite, power-type technology, applied in the direction of magnetic materials, inorganic materials, magnetic objects, etc., can solve the problems of high welding temperature, low material permeability, thermal shock resistance, weak mechanical strength, etc., to achieve The effect of strong operability and simple steps of the preparation method
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Embodiment 1
[0025] (1) The main material and auxiliary materials are weighed according to the proportion and mixed evenly to obtain the mixture. The specific proportion is shown in Table 1.
[0026] (2) The mixture is pre-fired in an oxidative atmosphere, the oxidative atmosphere is an air atmosphere, the pre-fire temperature is 800° C., and the holding time is 1 h.
[0027] (3) Grind the pre-fired mixture to the required particle size.
[0028] (4) Add an appropriate amount of binder to the sand-milled mixture for spray granulation and molding to obtain a green body.
[0029] (5) The green body is sintered and formed in an oxidative atmosphere to obtain a power type nickel-zinc ferrite material. The sintering temperature is 950° C. and the holding time is 2 hours.
Embodiment 2
[0031] (1) The main material and auxiliary materials are weighed according to the proportion and mixed evenly to obtain the mixture. The specific proportion is shown in Table 1.
[0032] (2) The mixture is pre-fired in an oxidative atmosphere, the oxidative atmosphere is an air atmosphere, the pre-fire temperature is 1050° C., and the holding time is 6 hours.
[0033] (3) Grind the pre-fired mixture to the required particle size.
[0034] (4) Add an appropriate amount of adhesive to the sand-milled mixed material to mechanically granulate and shape the material to obtain a green body.
[0035] (5) The green body is sintered in an oxidizing atmosphere to obtain a power type nickel-zinc ferrite material, the sintering temperature is 1200° C., and the holding time is 6 hours.
Embodiment 3
[0037] (1) The main material and auxiliary materials are weighed according to the proportion and mixed evenly to obtain the mixture. The specific proportion is shown in Table 1.
[0038] (2) The mixture is pre-fired in an oxidative atmosphere, the oxidative atmosphere is an air atmosphere, the pre-fire temperature is 1000° C., and the holding time is 2 hours.
[0039] (3) Grind the pre-fired mixture to the required particle size.
[0040] (4) Add an appropriate amount of adhesive to the sand-milled mixed material to mechanically granulate and shape the material to obtain a green body.
[0041] (5) The green body is sintered and formed in an oxidizing atmosphere to obtain a power-type nickel-zinc ferrite material. The sintering temperature is 1050° C. and the holding time is 3 hours.
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