A kind of penetrating agent for surface modification of nickel-based alloy and its application method
A surface modification, nickel-based alloy technology, applied in the direction of metal material coating process, coating, solid-state diffusion coating, etc., to achieve the effect of convenient operation, low cost, and improved high temperature and corrosion resistance
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Embodiment 1
[0035] Such as figure 1 As shown, the process of adopting the technical solution of the present invention is as follows: 1. Alkali washing: the DZ125 alloy sample is placed in a 65° C. alkali washing liquid for 15 minutes, and the alkali washing liquid is 100 g / L NaOH solution; 2. Water washing: Rinse the sample after alkali washing with running water and dry it; ③ Preparation of penetrating agent: Accurately weigh the penetrating agent according to the amount, and the proportion of Al-Y penetrating agent by weight percentage is: 12% Al, 7% NH 4 Cl (analytically pure), 1% Y 2 o 3 , the balance being Al 2 o 3 ; The proportion of Cr-Y penetration agent is by weight percentage: 15% Cr, 7% NH 4 Cl (analytically pure), 1% Y 2 o 3 , the balance being Al 2 o 3 ; ④ ball milling: place the prepared Al-Y osmotic agent and Cr-Y osmotic agent in a ball mill for grinding, make them fully mixed, and refine the osmotic agent particles; ⑤ drying: place the osmotic agent after ball mil...
Embodiment 2
[0037] Such as figure 1 As shown, the method flow process adopting the technical solution of the present invention is: 1. alkali washing: the DZ125 alloy sample is placed in a temperature of 70 ℃ of alkali washing liquid, soaked for 13min, and the alkali washing liquid is 20g / L Na 3 PO 4 solution; ②Water washing: rinse the sample after alkali washing with flowing water, and dry it; ③Preparation of osmotic agent: accurately weigh the osmotic agent according to the amount, and the proportioning of Al-Y osmotic agent is as follows: 10% Al, 6% NH 4 Cl (analytical pure), 1.5% Y 2 o 3 , the balance being Al 2 o 3 ; The proportion of Cr-Y penetration agent is by weight percentage: 10% Cr, 6% NH 4 Cl (analytical pure), 1.5% Y 2 o 3 , the balance being Al 2 o 3 ; ④ ball milling: place the prepared Al-Y osmotic agent and Cr-Y osmotic agent in a ball mill for grinding, make them fully mixed, and refine the osmotic agent particles; ⑤ drying: place the osmotic agent after ball mi...
Embodiment 3
[0039] Such as figure 1 As shown, the method flow for adopting the technical solution of the present invention is: 1. Alkali washing: the DZ125 alloy sample is placed in an alkali washing solution with a temperature of 80° C., soaked for 10 minutes, and the alkali washing solution is 75 g / L NaOH solution; 2. Water washing: Rinse the sample after alkali washing with running water and dry it; ③ Preparation of penetrating agent: accurately weigh the penetrating agent according to the amount, and the proportion of Al-Y penetrating agent is as follows: 15% Al, 10% NH 4 Cl (analytical pure), 2% Y 2 o 3 , the balance being Al 2 o 3 ; The proportion of Cr-Y penetration agent is by weight percentage: 18% Cr, 10% NH 4 Cl (analytical pure), 2% Y 2 o 3 , the balance being Al 2 o 3 ; ④ ball milling: place the prepared Al-Y osmotic agent and Cr-Y osmotic agent in a ball mill for grinding, make them fully mixed, and refine the osmotic agent particles; ⑤ drying: place the osmotic agen...
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