A kind of iron-silicon-ferrite composite magnetic core and its preparation method
A ferrite core and ferrite technology, applied in the direction of magnetic core/yoke, inductor/transformer/magnet manufacturing, magnetic objects, etc., can solve the problem of easy damage to switching power supply devices, increased reactive power consumption, difficult Play a role and other issues to achieve the effect of improving the power factor of the power supply, solving the transient current distortion, and protecting the electrical equipment
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[0030] The present invention also provides a method for preparing the iron-silicon-ferrite composite magnetic core described in the above technical solution, comprising the following steps:
[0031] (1) mixing the iron-silicon alloy powder with an insulating coating agent to obtain a mixed material;
[0032] (2) Molding the mixed material obtained in the step (1) with the ferrite core to obtain a green body;
[0033] (3) Preheating the green body obtained in the step (2) and then annealing to obtain an iron-silicon-ferrite composite magnetic core.
[0034] The invention mixes the iron-silicon alloy powder with the insulating coating agent to obtain the mixed material. In the present invention, the mixing temperature is preferably 15-130°C, more preferably 20-120°C, more preferably 40-100°C, most preferably 80-90°C; in the present invention, the mixing The speed is preferably 5-60r / min, more preferably 15-55r / min, more preferably 20-40r / min, most preferably 30r / min; in the pr...
Embodiment 1
[0043] 300 meshes of iron-silicon alloy powder with a weight of 28 grams, 1 g of phosphoric acid and 1 g of sodium silicate were mixed at room temperature for 10 minutes at a mixing rate of 5 to 60 r / min to obtain a mixed material; wherein the chemical composition of the iron-silicon alloy powder was Si 6.5% and The balance of Fe.
[0044] Put 12g of the mixed material into the mold of OD33.02mm×ID19.90mm×HT15mm, then put the nickel-zinc ferrite core with the mass of 3g and the size of OD30mm×ID25mm×HT3mm into the mold, and finally put the remaining Put 18g of mixed material into the mold, and the pressure reaches 21T / cm 2 Hold for 10s at the same time, and the green body is obtained by ejecting the mold;
[0045] The green body is preheated at 200°C for 50 minutes under the condition of vacuum degree of 0.08Pa to obtain the iron-silicon-ferrite composite magnetic core precursor;
[0046] Under the same vacuum condition, keep the temperature at 700°C for 60 minutes, and cool...
Embodiment 2
[0048] Mix 200-mesh iron-silicon alloy powder with a weight of 28.9 grams, 0.3 g tetraethyl orthosilicate and 0.8 g zinc stearate at a rate of 60 r / min at 80 ° C for 10 minutes to obtain a mixed material; the chemical composition of the iron-silicon alloy powder The composition is Si 6.5% and the balance Fe.
[0049] Put 20g of the mixed material into the mold of OD33.02mm×ID19.90mm×HT15mm, then put 3g of manganese zinc ferrite core with the size of OD30mm×ID25mm×HT3mm into the mold, and finally put the remaining 10g of the mixed material Put it into the mold, pressurize 20T / cm 2 Hold for 15s, withdraw from the mold, and obtain the green body;
[0050] In the condition of nitrogen with a flow rate of 5L / min, after preheating at 250°C for 80 minutes, in the same atmosphere, annealing at 680°C for 80 minutes to obtain a FeSi-Ferrite composite magnetic core.
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