A wallpaper gravure printing slurry capable of purifying indoor air and its preparation method and application
A gravure printing, inner air technology, applied in biocide-containing paints, antifouling/underwater coatings, coatings, etc., can solve the problems of efflorescence, water seepage, affecting the use effect of wallpaper and wall covering, and achieve color improvement , The effect of simple process steps and low equipment requirements
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Embodiment 1
[0028] (1) Preparation of air purification particles
[0029](1) Preparation of pretreated vermiculite powder: mix vermiculite powder, sodium hexametaphosphate and deionized water at a mass ratio of 1:0.03:200, stir and heat to 80°C, soak for 2 hours, stir at a speed of 1000r / min for 30 minutes, filter , dried to obtain dry vermiculite powder; add concentrated sulfuric acid to the dry vermiculite powder according to the mass ratio of 1:1, heat to 85 ° C for 3 hours, filter, wash with deionized water until the pH is neutral, dry, and calcined at 800 ° C , to obtain pretreated vermiculite powder;
[0030] (2) Preparation of composite carbon sol: furfural, water-soluble phenolic resin, carbon nanotubes, carboxymethyl cellulose, brucite fiber, sodium bicarbonate and deionized water in a mass ratio of 3:1:0.3:0.1:0.03 : 0.01: 100 mixed, mixed evenly, dripped ammonia water with a concentration of 0.25mol / L under stirring conditions, and the dropping rate was controlled at 10ml / min,...
Embodiment 2
[0038] (1) Preparation of air purification particles
[0039] (1) Preparation of pretreated vermiculite powder: mix vermiculite powder, sodium hexametaphosphate and deionized water at a mass ratio of 2:0.04:210, stir and heat to 85°C, soak for 3 hours, stir at a speed of 1200r / min for 35 minutes, filter , dried to obtain dry vermiculite powder; add concentrated sulfuric acid to the dry vermiculite powder according to the mass ratio of 1:1.5, heat to 87 ° C for 3 to 5 hours, filter, wash with deionized water until the pH is neutral, dry, and dry at 850 Calcined at ℃ to get pretreated vermiculite powder;
[0040] (2) Preparation of composite carbon sol: furfural, water-soluble phenolic resin, carbon nanotubes, carboxymethyl cellulose, brucite fiber, sodium bicarbonate and deionized water in a mass ratio of 4:1.5:0.4:0.12:0.04 : 0.02: 110 mixing, after mixing evenly, drip ammonia water with a concentration of 0.45mol / L under stirring conditions, the dropping rate is controlled a...
Embodiment 3
[0048] (1) Preparation of air purification particles
[0049] (1) Preparation of pretreated vermiculite powder: mix vermiculite powder, sodium hexametaphosphate and deionized water at a mass ratio of 3:0.05:220, stir and heat to 90°C, soak for 4 hours, stir at a speed of 1500r / min for 40 minutes, filter , dried to obtain dry vermiculite powder; add concentrated sulfuric acid to the dry vermiculite powder according to the mass ratio of 1:2, heat to 90 ° C for 5 hours, filter, wash with deionized water until the pH is neutral, dry, and calcined at 900 ° C , to obtain pretreated vermiculite powder;
[0050] (2) Preparation of composite carbon sol: furfural, water-soluble phenolic resin, carbon nanotubes, carboxymethyl cellulose, brucite fiber, sodium bicarbonate and deionized water in a mass ratio of 5:2:0.5:0.2:0.05 : 0.03: 120 mixed, mixed evenly, dripped ammonia water with a concentration of 0.75mol / L under stirring conditions, the dropping rate was controlled at 20ml / min, un...
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