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High-temperature and high-pressure multi-phase flow dynamic visualization loop corrosion testing apparatus and method thereof

A high-temperature, high-pressure, corrosion testing technology, applied in the direction of measuring devices, weather resistance/light resistance/corrosion resistance, instruments, etc., can solve the lack of shear force measurement devices, lack of online corrosion detection means, and inability to monitor the occurrence of corrosion on the surface of test pieces online and corrosion processes

Inactive Publication Date: 2016-12-21
SOUTHWEST PETROLEUM UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] (1) The method of stirring in the reactor is mainly used to simulate the corrosion effect of the flowing medium on the test piece, which cannot truly reflect the complex flow conditions and scouring effects of the multiphase flow medium in the pipeline;
[0006] (2) It is impossible to truly simulate the scouring damage effect of subcritical and supercritical fluids on the test piece;
[0007] (3) There is a lack of visualization devices, and there is little detailed research on the precipitation methods, conditions and forms of sulfur particles;
[0008] (4) Lack of shear force measurement device, unable to quantitatively analyze the erosion and damage effect of multiphase flow corrosion medium on corrosion inhibitor film and corrosion product film
[0009] (5) Lack of online corrosion detection means, unable to monitor the occurrence and process of corrosion on the surface of the test piece online;
[0010] (6) There is a lack of real-time recording means for experimental data, and relevant experimental data cannot be collected and processed in real time

Method used

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  • High-temperature and high-pressure multi-phase flow dynamic visualization loop corrosion testing apparatus and method thereof
  • High-temperature and high-pressure multi-phase flow dynamic visualization loop corrosion testing apparatus and method thereof
  • High-temperature and high-pressure multi-phase flow dynamic visualization loop corrosion testing apparatus and method thereof

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Embodiment

[0061] The invention is used to test the damage effect of multiphase flow acidic corrosive medium on equipment corrosion and erosion under different production conditions, and the experiment process is as follows:

[0062] Step 1: Install 1# arc test piece 34, 2# arc test piece 35, 3# arc test piece 36, 4# arc test piece 37 to corrosion test piece test device 31, inductance resistance probe 50, reference After the comparison electrode 51, the working electrode 52 and the counter electrode 53 are connected to the electrochemical signal detection device 30, the medium displacement unit 58 and the components on the circulation circuit 15 are connected and installed, and debugging is performed;

[0063] Step 2: Open 3# valve 3, N 2 Deoxidize through booster pump 8, 4# valve 4, 5# valve 5, 1# high temperature autoclave body 9, 6# valve 6, 7# valve 7, intake valve 14, circulation loop 15, exhaust valve 19 in turn , The time is 1h, then close the 3# valve 3; inject the liquid phase corros...

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Abstract

The invention discloses a high-temperature and high-pressure multi-phase flow dynamic visualization loop corrosion testing apparatus and a method thereof. The high-temperature and high-pressure multi-phase flow dynamic visualization loop corrosion testing apparatus comprises a medium displacement unit, an experiment parameter measurement unit, a visualization unit, a corrosion testing unit, a gas inlet valve, a circulation loop, a driving pump, a 1# end cover, a 2# end cover, a gas discharge valve and an H2S absorption device, wherein the experiment parameter measurement unit, the corrosion testing unit, the 1# end cover, the 2# end cover, the gas discharge valve and the H2S absorption device are arranged on the circulation loop, and the medium displacement unit is connected to the circulation loop through the driving pump. According to the present invention, the subcritical and supercritical fluids under the high-temperature and high-pressure environment can be realistically simulated, the shearing force can be measured, the erosion damage effect of the multi-phase flow corrosion medium on the corrosion inhibitor film and the corrosion product film can be quantitatively analyzed, and the online testing of the pipeline corrosion effect can be completed and the results are recorded.

Description

Technical field [0001] The invention relates to a high-temperature and high-pressure multiphase flow dynamic visual loop corrosion test device and method, and belongs to the technical field of petrochemical corrosion protection. Background technique [0002] With the continuous development of my country's oil and gas fields, more and more high-sulfur gas reservoirs have been discovered in China. The biggest difference between high-sulfur natural gas and conventional natural gas is the presence of hydrogen sulfide gas. In the development process of high-sulfur gas, as the gas pressure, temperature, and flow rate change, elemental sulfur will be precipitated in the gas. When elemental sulfur continues to accumulate and become so large that it cannot be carried away by the gas, sulfur deposition will occur. During the operation of surface pipelines, the different components and phases of the conveying medium have different degrees of erosion and corrosion on the surface pipelines a...

Claims

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Application Information

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IPC IPC(8): G01N17/02
CPCG01N17/02
Inventor 曾德智张恩搏喻智明董宝军施太和张智侯铎钟显康张乃艳
Owner SOUTHWEST PETROLEUM UNIV
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