Long-acting antimicrobial glass fiber air filtering paper and preparation method thereof
A technology of air filter paper and glass fiber, which is applied in the direction of filter paper, synthetic cellulose/non-cellulose material pulp/paper, filtration and separation, etc., which can solve the problem that nano silver and glass fiber cannot be tightly combined, the ventilation rate is large, and agglomeration is easy to occur and other problems, to achieve the effect of increasing the interaction area and interfacial bonding force, improving strength and stiffness, and excellent antibacterial properties
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Embodiment 1
[0023] A preparation method for antibacterial glass fiber air filter paper, comprising the steps of:
[0024] (1) Preparation of antibacterial glass fiber, comprising the following steps:
[0025] (1) Preparation of glass fiber: After crushing and mixing 54.4% SiO2, 15% B2O3, 0.6% Na2O, 12% Al2O3 and 18% CaO, put it in a 400mL corundum crucible, melt it with a silicon-molybdenum rod resistance furnace, and feed The temperature is 1370°C, the melting and clarification temperature is 1450±10°C, it is released at 1200°C, poured into a mold, sent into a muffle furnace, and annealed at 500°C to obtain glass; the prepared glass is heated to a drawing viscosity temperature of 1050 ℃, drawn into glass fibers of a specific diameter;
[0026] (2) Glass fiber pretreatment: After taking 45 parts of glass fiber for phase separation, carry out acid leaching treatment in 100ml of HCl solution with a concentration of 1mol / L. Dissolve the Na2O-B2O3 phase in acid, add 5ml of NH4Cl solution wi...
Embodiment 2
[0037] A preparation method for antibacterial glass fiber air filter paper, comprising the steps of:
[0038] (1) Preparation of antibacterial glass fiber, comprising the following steps:
[0039] (1) Preparation of glass fiber: After crushing and mixing 54.4% SiO2, 15% B2O3, 0.6% Na2O, 12% Al2O3 and 18% CaO, put it in a 400mL corundum crucible, melt it with a silicon-molybdenum rod resistance furnace, and feed The temperature is 1370°C, the melting and clarification temperature is 1450±10°C, it is released at 1200°C, poured into a mold, sent into a muffle furnace, and annealed at 500°C to obtain glass; the prepared glass is heated to a drawing viscosity temperature of 1050 ℃, drawn into glass fibers with a specific diameter;
[0040] (2) Glass fiber pretreatment: After taking 45 parts of glass fiber for phase separation, carry out acid leaching treatment in 100ml of HCl solution with a concentration of 1mol / L. Dissolve the Na2O-B2O3 phase in acid, add 5ml of NH4Cl solution wi...
Embodiment 3
[0051] A preparation method for antibacterial glass fiber air filter paper, comprising the steps of:
[0052] (1) Preparation of antibacterial glass fiber, comprising the following steps:
[0053] (1) Preparation of glass fiber: After crushing and mixing 54.4% SiO2, 15% B2O3, 0.6% Na2O, 12% Al2O3 and 18% CaO, put it in a 400mL corundum crucible, melt it with a silicon-molybdenum rod resistance furnace, and feed The temperature is 1370°C, the melting and clarification temperature is 1450±10°C, it is released at 1200°C, poured into a mold, sent into a muffle furnace, and annealed at 500°C to obtain glass; the prepared glass is heated to a drawing viscosity temperature of 1050 ℃, drawn into glass fibers with a specific diameter;
[0054] (2) Glass fiber pretreatment: After taking 45 parts of glass fiber for phase separation, carry out acid leaching treatment in 100ml of HCl solution with a concentration of 1mol / L. Dissolve the Na2O-B2O3 phase in acid, add 5ml of NH4Cl solution ...
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