Reverse osmosis concentrated water treatment method
A technology for reverse osmosis concentrated water and a treatment method, which is applied in the field of reverse osmosis concentrated water treatment and can solve the problems of high salt content, large solution chromaticity and high content of dissolved organic matter
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Embodiment 1
[0099] Embodiment 1: the preparation of 1# catalyst
[0100] Take 15g (about 50ml) of spherical alumina carrier from Shandong Zibo Wufeng Aluminum Magnesium Co., Ltd. and place it in a vacuum impregnation bottle for vacuum pretreatment. The vacuum pretreatment time is 30min and the vacuum degree is 96.0KPa; 0.15g / ml nickel nitrate aqueous solution 12ml, iron 0.10g / ml ferric nitrate aqueous solution 2.3ml, manganese 0.10g / ml manganese nitrate aqueous solution 3.0ml, cerium 0.15g / ml cerium nitrate aqueous solution 2.0ml, add into an ethanol aqueous solution with an ethanol concentration of 10 wt%, to prepare an immersion solution with a total volume of 25 ml. Add the above impregnation solution into the vacuum impregnation bottle equipped with the above spherical alumina carrier and mix evenly, then impregnate the above spherical alumina carrier with equal volume, after immersion for 30 minutes, take it out and dry it in an oven at 110°C for 3 hours, and then put it in the Calc...
Embodiment 2
[0102] Embodiment 2: the preparation of 2# catalyst
[0103] Take 15g (about 30ml) of spherical alumina carrier from Shandong Yantai Baichuan Huitong Technology Co., Ltd. and place it in a vacuum impregnation bottle for vacuum pretreatment. The vacuum pretreatment time is 30min and the vacuum degree is 98.0KPa; g / ml nickel nitrate aqueous solution 16ml, ferric nitrate aqueous solution 0.9ml containing iron 0.10g / ml, manganese nitrate aqueous solution 1.5ml containing manganese 0.10g / ml, cerium nitrate aqueous solution 2.5ml containing cerium 0.15g / ml, add to In deionized water, prepare an impregnation solution with a total volume of 21ml. Add the above impregnation solution into the vacuum impregnation bottle equipped with the above spherical alumina carrier and mix evenly, then impregnate the above spherical alumina carrier with an equal volume. After 60 min of impregnation, take it out and dry it in an oven at 130°C for 2 hours, and then put it in the Calcined at 480°C for ...
Embodiment 3
[0105] Embodiment 3: the preparation of 3# catalyst
[0106] Take 15g (about 30ml) of spherical alumina carrier from Shandong Yantai Baichuan Huitong Technology Co., Ltd. and place it in a vacuum impregnation bottle for vacuum pretreatment. The vacuum pretreatment time is 20min and the vacuum degree is 97.5KPa; Add 6.0ml of cerium nitrate aqueous solution per ml to the ethanol aqueous solution with ethanol concentration of 30wt%, and prepare an impregnation solution with a volume of 21ml, add the impregnation solution into a vacuum impregnation bottle and mix evenly, then impregnate the spherical alumina carrier with equal volume , after immersion for 30min, take it out and place it in an oven to dry at 120°C for 3h, and then bake it in a muffle furnace at 500°C for 4h to obtain a cerium-modified alumina carrier. In the obtained cerium-modified alumina carrier, the content of cerium is 2.0wt% based on the weight of alumina.
[0107] Take 15g (about 30ml) of the above-mentione...
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