Preparation method of waterborne antibacterial inorganic coating
An inorganic coating, water-based technology, applied in the field of coatings, can solve the problems of single function and difficult to meet multi-function, and achieve the effect of meeting multi-functional requirements, good antibacterial effect, excellent antibacterial and anti-formaldehyde characteristics
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Embodiment 1
[0030] A kind of preparation method of porous graphene loaded silver / titanium dioxide antibacterial composite material, it comprises the following steps:
[0031] (1) Preparation of graphene quantum dot suspension: weigh 0.5g of C60 powder, measure 100ml of concentrated sulfuric acid with a mass fraction of 98%, mix C60 powder and concentrated sulfuric acid in a beaker, put the beaker in an ice-water bath, and simultaneously Stir at a speed of 500rpm to obtain a mixed solution; weigh 3g of potassium permanganate powder, and slowly add it to the above mixed solution; remove the ice-water bath and replace it with a water bath, keep the temperature of the water bath at 30-40°C, and react for 5 hours; quickly add 200ml of pure Water, filtered, and then dialyzed for 3 days with a dialysis bag with a molecular weight cut-off of 1000 to obtain a suspension of graphene quantum dots; the suspension of graphene quantum dots was stirred at a speed of 100 rpm, while laser irradiation was p...
Embodiment 2
[0038] A kind of preparation method of porous graphene loaded silver / titanium dioxide antibacterial composite material, it comprises the following steps:
[0039] (1) Preparation of graphene quantum dot suspension: weigh 0.6g of C60 powder, measure 50-100ml of concentrated sulfuric acid with a mass fraction of 98%, mix C60 powder and concentrated sulfuric acid in a beaker, put the beaker in an ice-water bath, At the same time, stir at a speed of 500rpm to obtain a mixed solution; weigh 1g of potassium permanganate powder, and slowly add it to the above mixed solution; remove the ice-water bath and replace it with a water bath, keep the temperature of the water bath at 30~40°C, and react for 7 hours; quickly add 200ml of pure water, filtered, and then dialyzed with a dialysis bag with a molecular weight cut-off of 1000 for 3 days to obtain a suspension of graphene quantum dots; stir the suspension of graphene quantum dots at a speed of 100rpm, and irradiate the laser for 45min a...
Embodiment 3
[0046] A kind of preparation method of porous graphene loaded silver / titanium dioxide antibacterial composite material, it comprises the following steps:
[0047] (1) Preparation of graphene quantum dot suspension: Weigh 0.8g of C60 powder, measure 100ml of concentrated sulfuric acid with a mass fraction of 98%, mix C60 powder and concentrated sulfuric acid in a beaker, put the beaker in an ice-water bath, and simultaneously Stir at a speed of 500rpm to obtain a mixed solution; weigh 0.5g of potassium permanganate powder, and slowly add it to the above mixed solution; remove the ice-water bath and replace it with a water bath, keep the temperature of the water bath at 30-40°C, and react for 8 hours; quickly add 100ml Pure water, filtered, and then dialyzed for 3 days with a dialysis bag with a molecular weight cut-off of 1000, to obtain a suspension of graphene quantum dots; the suspension of graphene quantum dots was stirred at a speed of 100 rpm, while laser irradiation was p...
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