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Establishment method for UPLC fingerprint spectrum of gynecological reconstruction pill

A technology of gynecological reconstruction pills and fingerprints, which is applied in scientific instruments, measuring devices, instruments, etc., and can solve the problems that there are no gynecological reconstruction pills.

Active Publication Date: 2016-10-12
GUIYANG COLLEGE OF TRADITIONAL CHINESE MEDICINE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, there is no report on the research work on the ultra-high liquid fingerprint of Fuke Zaizao Pills

Method used

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  • Establishment method for UPLC fingerprint spectrum of gynecological reconstruction pill
  • Establishment method for UPLC fingerprint spectrum of gynecological reconstruction pill
  • Establishment method for UPLC fingerprint spectrum of gynecological reconstruction pill

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0071] A method for establishing the UPLC fingerprint of Fuke Zaizao Pills,

[0072] Prescription of Fuke Zaizao pills: 65.14g wine angelica, 65.14g vinegar cyperus, 43.43g white peony root, 21.71g rehmannia glutinosa, 10.86g donkey-hide gelatin, 65.14g poria cocos, 21.71g codonopsis, 21.71g astragalus, 32.57g yam, 16.28g Atractylodes macrocephala, Ligustrum lucidum 43.43g, Tortoise shell (burned with vinegar) 32.57g, Cornus officinalis 21.71g, Dipsacus 21.71g, Eucommia ulmoides 21.71g, Cistanche 10.86g, Raspberry 16.28g, Antler cream 5.43g, Rhizoma chuanxiong 43.43g, Salvia miltiorrhiza 21.71g , Achyranthes bidentata 16.28g, Motherwort 21.71g, Corydalis 16.28g, Sanqi (paste) 5.43g, Artemisia argyi (vinegar broiled) 43.43g, Cumin 21.71g, Ligusticum 21.71g, Sea octopus 32.57g, Burnet (vinegar Sunburn) 32.57g, Yizhi 10.86g, Alisma 21.71g, lotus leaf (vinegar roast) 16.28g, Gentiana 21.71g, Digupi 21.71g, Baiwei 43.43g, Chunpi 32.57g, amber 5.43g, wine skullcap 32.57g, Suanzaore...

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Abstract

The invention discloses an establishment method for a UPLC fingerprint spectrum of a gynecological reconstruction pill. According to the method, the authenticity and merits of the product can be quickly and accurately identified, and the advantages of being easy and convenient to use, stable, high in precision, good in reproducibility and the like are achieved; in addition, the variety and number of chemical components contained in the gynecological reconstruction pill can be comprehensively reflected, then the quality of the gynecological reconstruction pill is integrally described and evaluated, therefore, the quality and the medicine effect of the gynecological reconstruction pill can be truly combined together, illumination of the action mechanism is promoted, and a basis is provided for technology improvement and deep development of the gynecological reconstruction pill. Furthermore, the fingerprint spectrum, detected through the method, of the gynecological reconstruction pill contains relatively more chemical components and is moderate in height proportion of all characteristic peaks, stable in base line and good in separation degree, peak shape and column efficiency.

Description

technical field [0001] The invention relates to a method for establishing UPLC fingerprints of gynecological Zaizao pills, belonging to the field of pharmaceutical technology. Background technique [0002] Fuke Zaizao Pill is a well-known medicine for treating gynecological diseases. It is composed of 42 authentic medicinal materials. It has the effects of nourishing blood and regulating menstruation, nourishing liver and kidney, warming the uterus and relieving pain. Bleeding, dysmenorrhea, leukorrhea embolism. [0003] Fuke Zaizao Pills were developed from traditional Chinese medicine ancient prescriptions. Due to the limitation of scientific research level at that time, the starting point of its quality standard was not high enough, and basic research on pharmacology and drug effects was relatively limited. In order to further explore its mechanism of action and medicinal basis, and ensure product safety, effectiveness, and quality control, it is urgent to use modern med...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/02
CPCG01N30/02G01N2030/027
Inventor 徐剑张永萍杨立勇缪艳燕刘耀
Owner GUIYANG COLLEGE OF TRADITIONAL CHINESE MEDICINE
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