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Sea mud/plant composite bacteria inhibiting and whitening polypropylene fibers and preparation method thereof

A polypropylene fiber and polypropylene resin technology is applied in the field of sea mud/plant composite antibacterial and whitening polypropylene fiber and its preparation. The effect of enhancing the stability, preventing agglomeration, improving the interface polarity and chemical microenvironment

Inactive Publication Date: 2016-09-28
陆建益
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, because there are a large number of inorganic ions in the sea mud layer, it shows hydrophilic and oleophobic properties, and the spacing is small, which makes it difficult to insert organic macromolecular chains, which greatly limits its application.
A large number of patent documents and published research papers have been searched, and the use of sea mud-loaded plant extracts as antibacterial and whitening agents in polypropylene fibers has not been found at home and abroad so far.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] 1. Raw material pretreatment:

[0033] ① Preparation of sea mud powder: collect a certain amount of sea mud, add water to prepare mud with a solid content of 50%, add 0.9% of sea mud weight dithiocarbamate and stir evenly, then add citric acid to adjust the pH value To 3.5, keep stirring at 50°C for 3 hours, let it stand for 24 hours, discard the bottom sediment, pour out the upper slurry, filter, and wash the obtained solid with deionized water for 3 times, bake at 100°C for 9 hours, and pulverize , through a 70-mesh sieve to obtain sea mud powder;

[0034] ② Preparation of Italian Buglossia extract: Collect dried Italian Buglossia, wash and dry, add 12 times the weight of Italian Buglossia to it, boil for 3 hours at 100°C, filter, and cool the filtrate to room temperature. Adding ethanol with a concentration of 90wt% at a weight ratio of 1:1, airtightly refrigerating at 0° C. for 13 hours, filtering, evaporating and concentrating the water and ethanol in the filtrate...

Embodiment 2

[0045] 2. Raw material pretreatment:

[0046]①Preparation of sea mud powder: collect a certain amount of sea mud, add water to prepare mud with a solid content of 50%, and add dithiocarbamate with a weight of 1.2% of sea mud and stir evenly, then add citric acid to adjust the pH value To 4.5, keep stirring and reacting at 65°C for 1.5h, let it stand for 24h, discard the bottom sediment, pour out the upper layer slurry, filter, and repeatedly wash the obtained solid with deionized water for 3 times, and bake at 100°C for 7h, Pulverize, cross 80 mesh sieves, obtain sea mud powder;

[0047] ②Preparation of Italian Buglossia extract: Collect dried Italian Buglossia, wash and dry, add water 15 times the weight of Italian Buglossia, boil at 100°C for 1.5h, filter, and cool the filtrate to room temperature , adding ethanol with a concentration of 95wt% at a weight ratio of 1:1, airtightly refrigerating at 2°C for 16h, filtering, evaporating and concentrating the water and ethanol in...

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PUM

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Abstract

The invention provides sea mud / plant composite bacteria inhibiting and whitening polypropylene fibers and a preparation method thereof. The polypropylene fibers are prepared from the following components by weight percent: 70-98% of polypropylene resin, 1-25% of bacteria inhibiting and whitening master batch, 0.8-3% of cerasus humilis kernel, 0.1-1.5% of magnesium ascorbyl phosphate and 0.1-0.5% of di-iso-octyldiphenylamine, wherein the bacteria inhibiting and whitening master batch comprises the following raw materials by weight percent: 65-90% of polypropylene resin, 5.9-25% of sea mud powder, 2.5-5% of anchusa italica extract, 1.5-3.5% of extract of root of wintersweet and 0.1-1.5% of coupling agent. The polypropylene fibers prepared by reasonably compounding the raw materials by various processing means have fragrant smell, good skin affinity, hygroscopicity, spinnability and dyeing property and high fiber forming strength, not only have a wide antibacterial spectrum, good antibacterial effects and lasting effects but also show the effect of inhibiting skin pigmentation and the effects of whitening and beautifying and conduce to improving human health when frequently coming into contact with the skins of human bodies.

Description

technical field [0001] The invention relates to the technical field of textiles, in particular to a sea mud / plant composite antibacterial and whitening polypropylene fiber and a preparation method thereof. Background technique [0002] Polypropylene fiber, also known as PP fiber or polypropylene fiber. It is a synthetic fiber spun from isotactic polypropylene obtained by propylene polymerization. Because of its simple production process, low price, light relative density, high strength, corrosion resistance, mildew resistance, good resilience, and good fabric effect, it is unique in the application of textiles that live with the human body day and night. It is used to make underwear , swimwear, socks, bed sheets and other textiles that are in close contact with the human body and one of the best fibers for medical and sanitary nonwovens. However, polypropylene fiber also has certain defects, such as not easy to dye, poor hygroscopicity, air permeability and drapability, et...

Claims

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Application Information

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IPC IPC(8): D01F6/46D01F1/10
CPCD01F6/46D01F1/103
Inventor 陆建益
Owner 陆建益
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