Method for preparing nano-crystalline cellulose of flexible screen matrix material
A technology of nanocellulose and matrix materials, applied in the field of preparation of nanocellulose used in flexible screen matrix materials, can solve the problems of efficiency, life, process operability, insufficient cost, slow degradation, etc., and achieve environmental protection and waste disposal effects on object disposal, good biodegradability
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Embodiment 1
[0014] A preparation method of nanocellulose used in a flexible screen matrix material:
[0015] Using unbleached bagasse pulp and chitosan as raw materials, first dissolve the unbleached bagasse pulp in water and break it up to make a suspension, and then add a mixture of sulfuric acid and trifluoroacetic acid with a weight ratio of 30:1 to it. Acids are mixed and reacted to form a highly crystalline suspension. After centrifugation, the solid matter is washed, and then treated with a high-pressure ultrasonic homogenizer to obtain a nanocellulose crystal suspension slurry, and potassium periodate is added to the suspension slurry for oxidation treatment to obtain a modified nanocellulose suspension slurry. The chitosan raw material was treated with acetic acid at a low temperature of 3°C to make a chitosan saturated solution, and then subjected to ultrasonic atomization and freezing to obtain nano-scale chitosan. The nano-scale chitosan is mixed with the modified nano-cellul...
Embodiment 2
[0017] A preparation method of nanocellulose used in a flexible screen matrix material:
[0018] Using bagasse unbleached pulp and chitosan as raw materials, first dissolve the bagasse unbleached pulp in water and break it up to make a suspension, and then add a mixture of sulfuric acid and trifluoroacetic acid at a weight ratio of 30:1.1 Acids are mixed and reacted to form a highly crystalline suspension. After centrifugation, the solid matter is washed, and then treated with a high-pressure ultrasonic homogenizer to obtain a nanocellulose crystal suspension slurry, and potassium periodate is added to the suspension slurry for oxidation treatment to obtain a modified nanocellulose suspension slurry. The chitosan raw material was treated with acetic acid at a low temperature of 5°C to make a chitosan saturated solution, and then subjected to ultrasonic atomization and freezing to obtain nano-scale chitosan. The nano-scale chitosan is mixed with the modified nano-cellulose sus...
Embodiment 3
[0020] A preparation method of nanocellulose used in a flexible screen matrix material:
[0021] Using unbleached bagasse pulp and chitosan as raw materials, first dissolve the unbleached bagasse pulp in water and break it up to make a suspension, and then add a mixture of sulfuric acid and trifluoroacetic acid at a weight ratio of 30:1.2 Acids are mixed and reacted to form a highly crystalline suspension. After centrifugation, the solid matter is washed, and then treated with a high-pressure ultrasonic homogenizer to obtain a nanocellulose crystal suspension slurry, and potassium periodate is added to the suspension slurry for oxidation treatment to obtain a modified nanocellulose suspension slurry. The chitosan raw material was treated with acetic acid at a low temperature of 7°C to make a saturated solution of chitosan, and then subjected to ultrasonic atomization and freezing to obtain nano-scale chitosan. The nano-scale chitosan is mixed with the modified nano-cellulose ...
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