Method for preparing silica sol in tubular slurry reactor
A slurry reactor, tube-and-tube technology, applied in chemical instruments and methods, silicon compounds, inorganic chemistry, etc., can solve problems such as uneven heating
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Embodiment 1
[0022] A method for preparing silica sol in a tubular slurry reactor, its components are calculated in parts by mass, comprising the following process steps:
[0023] The particle size of silicon powder is 100 mesh, and the addition amount is 20 parts, added in 4 times; the lye is composed of 0.5 parts of KOH and 99.5 parts of water. The height of the reactor is 0.7m, and it is formed by arranging 6 slurry reaction tubes with an inner diameter of 14mm. The aspect ratio is 50:1. The outer diameter of the slurry reactor is 0.06m; the reaction temperature is 50°C, and the reaction time is 2 hours. The particle size of the obtained silica sol was 14 nm. image 3 A scanning electron microscope of silica sol was obtained for this example.
Embodiment 2
[0025] A method for preparing silica sol in a tubular slurry reactor, its components are calculated in parts by mass, comprising the following process steps:
[0026] The particle size of the silicon powder is 300 mesh, and the addition amount is 60 parts, added in 5 times; the lye consists of 0.5 parts of KOH, 0.5 parts of NaOH and 99 parts of water. The height of the reactor is 5m, and it is formed by arranging 60 slurry reaction tubes with an inner diameter of 20mm. The aspect ratio is 250:1. The outer diameter of the slurry reactor is 0.15m; the reaction temperature is 65°C, and the reaction time is 12 hours. The particle size of the obtained silica sol was 32 nm. Figure 4 A scanning electron microscope of silica sol was obtained for this example.
Embodiment 3
[0028] A method for preparing silica sol in a tubular slurry reactor, its components are calculated in parts by mass, comprising the following process steps:
[0029] The particle size of the silicon powder is 300 mesh, and the addition amount is 40 parts, added in 4 times; the lye is composed of 0.5 parts of NaOH and 99.5 parts of water. The height of the reactor is 4m, and it is formed by arranging 14 slurry reaction tubes with an inner diameter of 50mm. The aspect ratio is 80:1, and the outer diameter of the slurry reactor is 0.5m; the reaction temperature is 90°C, and the reaction time is 10 hours. The particle size of the obtained silica sol was 21 nm. Figure 5 A scanning electron microscope of silica sol was obtained for this example.
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