Device and method for improving production efficiency of titanium sponge and reducing energy consumption
A technology of production efficiency and sponge titanium, which is applied in the field of rare metal metallurgy to achieve the effect of increasing the distillation speed, shortening the distillation cycle, and reducing the cost of electricity consumption.
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Embodiment 1
[0062] as above about figure 1 and figure 2 Introduction, in this embodiment, preferably the bottom end of the fusible columnar body 7 is stable on the sieve plate plane, and is supported by the sieve plate; 7-n are vertically stacked and combined, and the constituent material of each fusible short columnar body 7-n is metal magnesium material.
[0063] In this embodiment, the fusible columnar body 7 is a hollow cylinder, and the hollow cylinder passes through its inner hole 8 and fits on the central positioning column 9 fixedly placed on the axis of the reactor 5; the diameter of the central positioning column 9 is 100mm, and the center The height of the positioning column 9 is slightly below the upper cover of the reactor, and the material of the central positioning column is 904L; the inner diameter of the hollow cylinder 7 (meltable column 7) is 120mm, and the hollow cylinder 7 (meltable column 7 ) is 300mm in outer diameter, the height of the fusible short hollow cylin...
Embodiment 2
[0075] Such as figure 1 As shown, the difference between this embodiment and embodiment 1 is that the substance constituting the meltable columnar body 7 is magnesium chloride. During the reduction process, through the melting and endothermic effect of the magnesium chloride soluble columnar body 7, the heat accumulated in the central area of the liquid metal magnesium is eliminated, and the formation of a large amount of low-valent titanium and free titanium powder caused by the high-temperature vaporization of the metal magnesium is avoided. It also avoids the sintering phenomenon of titanium crystal caused by the high temperature in the central region of liquid metal magnesium, and also improves the efficiency of magnesia thermal reduction. Refer to Example 1 for other parts of this example.
Embodiment 3
[0077] Such as image 3 As shown, the difference between this embodiment and Embodiment 1 is that the fusible columnar body 7 consists of two kinds of metal magnesium fusible short hollow cylinders 7-1 and magnesium chloride fusible short hollow cylinders 7-1 with different constituent materials. 2 staggered superimposed composition, wherein: the height of metal magnesium fusible short hollow cylinder 7-1 is 800 mm, and the height of magnesium chloride short fusible hollow cylinder 7-2 is 200 mm. Refer to Example 1 for other parts of this example.
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