Preparation method for silver-iron-rhenium electric contact material
An electrical contact material and silver-iron technology, which is applied in the field of preparation of silver-iron-rhenium electrical contact materials, can solve problems such as difficulty in producing silver-iron-rhenium alloys, and achieve the effects of improving processing performance, electrical contact performance and uniform distribution.
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Embodiment 1
[0029] Embodiment 1, a preparation method of a silver-iron-rhenium electrical contact material. Its specific method is as follows:
[0030] a. Powder mixing: 7.6 parts by mass of 99.99% high-purity ammonium rhenate and 92.4 parts by mass of 99.95% carbonyl iron powder were mixed with a V-type powder mixer for 60 hours at a speed of 60 rpm;
[0031] b. Roasting: The mixed powder is roasted and decomposed at a temperature of 400°C, and its reaction formula is:
[0032] 2NH 4 ReO 4 → Re 2 o 7 +2NH 3 ↑+H 2 0↑
[0033] 3Fe+2O 2 → Fe 3 o 4
[0034] c. Reduction: the mixed powder of iron oxide and rhenium iron oxide is passed into hydrogen protection for reduction, the reduction temperature is 1000 ° C, and the time is 1 hour to obtain 70.05 parts by mass of iron-rhenium alloy powder containing 94.915% iron and 5.085% rhenium. The reaction formula :
[0035] Re 2 o 7 +7H 2 →2Re+7H 2 0↑
[0036] Fe 3 o 4 +3H 2 →3Fe+4H 2 0↑
[0037] d. Ball milling and sieving: A...
Embodiment 2
[0046] Embodiment 2, a preparation method of a silver-iron-rhenium electrical contact material. Its specific method is as follows:
[0047] a, powder mixing: 1.564 kg of 99.99% high-purity ammonium rhenate and 18.983 kg of 99.95% carbonyl iron powder were mixed with a V-type powder mixer for 48 hours at a speed of 80 rpm;
[0048] b. Roasting: The mixed powder is roasted and decomposed at a temperature of 450°C, and its reaction formula is:
[0049] (NH 4 ) 2 ReO 4 → Re 2 o 7 +2NH 3 ↑+H 2 0↑
[0050] 3Fe+2O 2 → Fe 3 o 4
[0051]c. Reduction: The mixed powder of iron oxide and rhenium iron oxide is passed into hydrogen protection for reduction. The reduction temperature is 1250 ° C and the time is 3 hours to obtain 20 kg of iron-rhenium alloy powder containing 94.915% iron and 5.085% rhenium. The reaction formula :
[0052] Re 2 o 7 +7H 2 →2Re+7H 2 0↑
[0053] Fe 3 o 4 +3H 2 →3Fe+4H 2 0↑
[0054] d. Ball milling and sieving: After the powder is cooled, g...
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