Preparation method of breast-milk patterned structured oil and breast-milk patterned structured oil prepared by preparation method and use of breast-milk patterned structured oil
A technology of structured oils and fats, applied in dairy products, applications, milk preparations, etc., can solve the problems of difficult large-scale application and high cost, and achieve the effects of easy absorption, control of production costs, and large-scale industrial production
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[0077] (1) The preparation method of the present invention uses edible oils of natural origin as raw materials. Because the raw materials of edible oils are widely available, and compared to using commercially available processed products (such as oleic acid, etc.) as raw materials In terms of cost, the cost is lower, which enables the production cost to be significantly reduced when preparing breast-emulsion structured grease according to the method of the present invention, improves the profit margin of the product, and brings good economic benefits to the production enterprise.
[0078] (2) In the preparation method of the present invention, the random transesterification reaction and the directional transesterification reaction are combined, so as to realize the preparation of the desired breast-emulsion structured fat with a simple and controllable process. At the same time, because the above-mentioned process is simple and controllable, it is more conducive to the production...
Embodiment 1
[0087] The palm oil fraction with IV=8 and coconut oil are placed in a reactor at a mass ratio of 3:1 and mixed uniformly to obtain a mixed fat. The mixed grease is vacuum dried at 105° C. for 30 minutes to remove the moisture therein and obtain a dried mixed grease. Then, the dried mixed fat is kept at a temperature of 100° C., 0.3 wt% of sodium methoxide is added thereto, and a random transesterification reaction is performed under vacuum conditions. After the transesterification reaction was carried out for 0.1 h, an aqueous solution of citric acid was added to terminate the reaction to obtain a reaction product. The reaction product was fully shaken and mixed and centrifuged, and then the upper oil phase obtained by centrifugation was washed with distilled water to neutrality and dried under vacuum for 30 minutes, and finally decolorized and deodorized (at a temperature of 110 ℃, 8mmHg Add 1.0wt% of the white clay by weight of the reaction product and decolorize for 20 min...
Embodiment 2
[0091] The palm oil fraction with IV=30 and MCT were placed in a reactor at a mass ratio of 5:1 and mixed uniformly to obtain a mixed fat. With respect to the total weight of the obtained mixed oil and fat, 8 wt% of lipase Lipozyme TLIM was added to the mixed oil and fat, and the transesterification reaction was performed at 65° C. for 8 h. The lipase is removed by filtration to obtain a reaction product. The reaction product was processed through the decolorization and deodorization refining operations described in Example 1 to obtain refined random transesterified fats and oils.
[0092] The sunflower oil and olive oil are mixed at a mass ratio of 1:1 to obtain a mixed vegetable oil. Subsequently, NaOH and distilled water were added to the mixed vegetable oil to carry out a hydrolysis reaction, and the mixture was refluxed and condensed at 75° C. for 1 hour to obtain the product. Subsequently, the product was placed at room temperature for cooling, distilled water and n-hexan...
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