Polyionic liquid type acid indicator suitable for non-polar solvent and its preparation
A technology of polyionic liquids and non-polar solvents, which is applied in the direction of material analysis by observing the influence on chemical indicators, and analysis by making materials undergo chemical reactions, etc., to achieve simple synthesis, good reaction controllability, and good thermal stability. The effect of stability
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Embodiment 1
[0043] A polyionic liquid acid indicator suitable for non-polar solvents, its structural formula is shown in formula (3), wherein, n is 22.
[0044] The preparation method of the above-mentioned polyionic liquid type alkaline indicator suitable for non-polar solvents is:
[0045] Step a: Carry out water and oxygen removal treatment on a 150 ml three-necked flask. The water and oxygen removal treatment is as follows: fully dry the clean 150 ml three-necked flask at 90 degrees Celsius for 3 hours, take it out and cool it to room temperature, and inject nitrogen gas ;
[0046] Step b: under nitrogen protection, add 29.60 g of phthalic anhydride and 50 ml of N,N-dimethylformamide into the three-necked flask, and stir to form a uniform solution;
[0047] Step c: Add 0.13 grams of ethylene glycol (accounting for 1% by mole of phthalic anhydride) to the solution obtained in step b under nitrogen protection, and stir;
[0048] Step d: add 18.50 g of epichlorohydrin to the solution o...
Embodiment 2
[0054] A polyionic liquid type acid indicator suitable for non-polar solvents, its structural formula is shown in formula (3), wherein, n is 17.
[0055] The preparation method of the above-mentioned polyionic liquid type alkaline indicator suitable for non-polar solvents is:
[0056] Step a: Carry out water and oxygen removal treatment on a 150 ml three-necked flask. The water and oxygen removal treatment is as follows: fully dry the clean 150 ml three-necked flask at 90 degrees Celsius for 3 hours, take it out and cool it to room temperature, and inject nitrogen gas ;
[0057] Step b: under nitrogen protection, add 28.00 g of phthalic anhydride and 50 ml of N,N-dimethylformamide into a three-necked flask, and stir to form a uniform solution;
[0058] Step c: add 0.15 grams of ethylene glycol (accounting for 1.2% mole percent of phthalic anhydride) to the solution obtained in step b under nitrogen protection, and stir;
[0059] Step d: add 17.50 g of epichlorohydrin to the ...
Embodiment 3
[0065] A polyionic liquid type acid indicator suitable for non-polar solvents, its structural formula is shown in formula (3), wherein, n is 24.
[0066] The preparation method of the above-mentioned polyionic liquid type alkaline indicator suitable for non-polar solvents is:
[0067] Step a: Carry out water and oxygen removal treatment on a 150 ml three-necked flask. The water and oxygen removal treatment is as follows: fully dry the clean 150 ml three-necked flask at 90 degrees Celsius for 3 hours, take it out and cool it to room temperature, and inject nitrogen gas ;
[0068] Step b: under nitrogen protection, add 25.50 g of phthalic anhydride and 50 ml of N,N-dimethylformamide into a three-necked flask, and stir to form a uniform solution;
[0069] Step c: add 0.2 grams of ethylene glycol (accounting for 1.8% by mole of phthalic anhydride) to the solution obtained in step b under nitrogen protection, and stir;
[0070] Step d: Add 15.90 g of epichlorohydrin to the soluti...
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