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Nano aluminum-platinum catalyst and applications thereof

A platinum catalyst and nano-aluminum technology, which is applied in the field of preparation of pyridine derivatives, can solve the problems of unsuitability for large-scale industrial production, high cost of raw materials, lack of catalysts, etc., and achieve the effect of reasonable design, less pollution to the environment, and improved surface activity

Active Publication Date: 2015-12-23
ANHUI XINGYU CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0011] Aiming at the problems of high raw material cost, low yield, unsuitability for large-scale industrial production, and lack of suitable catalysts in the existing preparation methods of 2-pyridinemethanol, the present invention provides a nano-aluminum platinum catalyst and its application, which can Reduce the preparation cost of 2-pyridinemethanol, increase the yield, and have little pollution

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] First prepare a catalyst, a nano-aluminum-platinum catalyst, consisting of platinum powder and aluminum powder, the mass ratio of the platinum powder to aluminum powder is 1:8.5, the size of the platinum powder is 5nm, and the size of the aluminum powder is 4.0nm.

[0026] A kind of preparation method of nano aluminum platinum catalyst, its step:

[0027] (1) Grinding metal platinum into platinum powder with a size of 5nm, and grinding metal aluminum into aluminum powder with a size of 4.0nm;

[0028] (2) the platinum powder and the aluminum powder in the step (1) are mixed evenly according to the ratio of 1:8.5 according to the mass ratio, to obtain the mixed powder;

[0029] (3) compressing the mixed powder in step (2) with a tablet press, with a pressure of 137N, to obtain a mixed briquette;

[0030] (4) The mixed briquette in step (3) was placed in an aqueous sodium hydroxide solution with a mass concentration of 29% for 2 minutes to obtain a finished catalyst. Th...

Embodiment 2

[0032] Same as Example 1, the difference is that the size of the platinum powder is 3.5nm, and the size of the aluminum powder is 4.5nm. The prepared finished catalyst is loose and porous, with a density of 0.28g / cm 3 .

Embodiment 3

[0034] Same as Example 1, the difference is that the size of the platinum powder is 7nm, and the size of the aluminum powder is 3.0nm. The prepared finished catalyst is loose and porous, with a density of 0.39g / cm 3 .

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Abstract

The invention relates to a nano aluminum-platinum catalyst, a manufacturing method and applications thereof, and a preparation method of 2-pyridine methanol. The application number of divisional application is 201410149195.6. The application date is April 14th, 2014. The invention discloses a nano aluminum-platinum catalyst, a preparation method and applications thereof, and belongs to the field of preparation of pyridine derivatives. The provided nano aluminum-platinum catalyst is composed of platinum powder and aluminum powder according to a weight ratio of 1:8.5; wherein the size of platinum powder is 3.5 to 7 nm, and the size of aluminum powder is 3.0 to 4.5 nm. The preparation method of 2-pyridine methanol comprises two parts, has the advantages of simple materials, reasonable design, and little environment pollution, and is carried out in the presence of a special catalyst. The synthesis is very simple, and the second step in synthesis can be performed at a room temperature under a normal pressure.

Description

[0001] This application is a divisional application of an invention patent titled: a nano-aluminum platinum catalyst, its manufacturing method, application, and 2-pyridinemethanol, and its application number is: 201410149195.6. The filing date of the parent application is April 14, 2014 day. technical field [0002] The invention belongs to the field of preparation of pyridine derivatives, in particular, relates to a nano-aluminum-platinum catalyst and its application, more specifically, relates to a novel nano-aluminum and platinum catalyst for 2-pyridinemethanol and its application. Background technique [0003] With the development of economy and society, there is an increasing demand for various raw materials in industry, especially pyridinemethanol is widely used as an intermediate of pesticides and medicines. At present, there are following 4 methods for synthesizing pyridinemethanol from different raw materials: [0004] (1) bromination method, after the bromination ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J23/42C07D213/30B82Y30/00B82Y40/00
Inventor 张宽宇金文艺丁亮张昊张升
Owner ANHUI XINGYU CHEM
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