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Bismuth-oxide-based black pigment used for glass digital inkjet printing and preparation method of bismuth-oxide-based black pigment

A technology of digital inkjet and black coloring material, which is applied in applications, household utensils, ink, etc., can solve the problems that restrict product development, and achieve the effects of strong market adaptability, simple and efficient preparation method, and low sintering temperature

Inactive Publication Date: 2015-11-18
JIANGSU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, so far, there is no bismuth oxide-based black colorant and its preparation method for glass digital inkjet printing with independent intellectual property rights in my country, which restricts my country's glass digital inkjet printing technology and its products to a certain extent. development of

Method used

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  • Bismuth-oxide-based black pigment used for glass digital inkjet printing and preparation method of bismuth-oxide-based black pigment
  • Bismuth-oxide-based black pigment used for glass digital inkjet printing and preparation method of bismuth-oxide-based black pigment
  • Bismuth-oxide-based black pigment used for glass digital inkjet printing and preparation method of bismuth-oxide-based black pigment

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Experimental program
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Effect test

Embodiment 1

[0029] A bismuth oxide-based black colorant for glass digital inkjet printing, the preparation method of which is as follows:

[0030] First of all, for a 500ml ball mill tank, it is suitable to grind 25g of black pigment at a time, according to bismuth oxide (α-type Bi 2 o 3 ) 37.95%, amorphous silicon oxide (SiO 2 ) 15%, boron oxide (B 2 o 3 )6.8%, lithium oxide (Li 2 O) 4.3%, alumina (Al 2 o 3 )2.75%, zirconia (ZrO 2 ) 1.2%, copper chrome black 32% mass percent, calculate each raw material quality that ball milling 25g black pigment needs, bismuth oxide (alpha-type Bi 2 o 3 ) 9.49 g, amorphous silicon oxide (SiO 2 ) 3.75 grams, boron oxide (B 2 o 3 ) 1.7 g, lithium oxide (Li 2 O) 1.08 grams, aluminum oxide (Al 2 o 3 ) 0.68 g, zirconia (ZrO 2 ) 0.3 grams, copper chrome black 8 grams, then weighed according to the calculation results;

[0031] Secondly, put the weighed raw materials in a beaker, stir evenly, and then weigh 196g of agate balls according to the ...

Embodiment 2

[0037] The experimental method of this embodiment is similar to that of the first embodiment, except that the mass percentages of the raw materials are different. According to bismuth oxide (α-type Bi 2 o 3 ) 32.95%, amorphous silicon oxide (SiO 2 ) 13%, boron oxide (B 2 o 3 )4.8%, lithium oxide (Li 2 O) 3.3%, alumina (Al 2 o 3 ) 2.25%, zirconia (ZrO 2 ) 1%, the mass percentage of copper chromium black 42.7%, calculate the required raw material quality of ball milling 25g black ink powder color material, bismuth oxide (α-type Bi 2 o 3 ) 8.2 g, amorphous silicon oxide (SiO 2 ) 3.25 grams, boron oxide (B 2 o 3 ) 1.2 g, lithium oxide (Li 2 O) 0.83 g, alumina (Al 2 o 3 ) 0.56 g, zirconia (ZrO 2 ) 0.25 gram, copper chrome black 10.71 gram, weigh according to calculation result then, following steps are completely consistent with embodiment 1.

[0038] The black pigment that present embodiment obtains, and figure 1 Similar, compared with Example 1, the finished blac...

Embodiment 3

[0040] The experimental method of this embodiment is similar to that of the first embodiment, except that the mass percentages of the raw materials are different. According to bismuth oxide (α-type Bi 2 o 3 ) 42.95%, amorphous silicon oxide (SiO 2 ) 17%, boron oxide (B 2 o 3 )8.8%, lithium oxide (Li 2 O) 5.3%, alumina (Al 2 o 3 )3.25%, zirconia (ZrO 2 ) 1.4%, copper chromium black 21.3% mass percent, calculate the required each raw material quality of ball milling 25g black ink powder color material, bismuth oxide (α-type Bi 2 o 3 ) 10.7 g, amorphous silicon oxide (SiO 2 ) 4.25 grams, boron oxide (B 2 o 3 ) 2.2 g, lithium oxide (Li 2 O) 1.33 grams, aluminum oxide (Al 2 o 3 ) 0.81 g, zirconia (ZrO 2 ) 0.35 gram, copper chrome black 5.36 gram, weigh according to calculation result then, following steps are completely consistent with embodiment 1.

[0041] The black pigment that present embodiment obtains, and figure 1 Similar, compared with Example 1, the finish...

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Abstract

The invention provides bismuth-oxide-based black pigment used for glass digital inkjet printing and a preparation method of the bismuth-oxide-based black pigment. The bismuth-oxide-based black pigment is characterized in that preparation raw materials of the bismuth-oxide-based black pigment include bismuth oxide (alpha type Bi2O3), amorphous state silicon oxide (SiO2), boron oxide (B2O3), lithium oxide (LiO2), aluminum oxide (Al2O3), zirconium oxide (ZrO2) and copper chromite black (common industrial coloring materials); the preparation method includes the steps of evenly mixing bismuth oxide (alpha type Bi2O3), amorphous state silicon oxide (SiO2), boron oxide (B2O3), lithium oxide (LiO2), aluminum oxide (Al2O3) and zirconium oxide (ZrO2), conducting high energy ball milling to make the mixture sufficiently and mechanically alloyed, and mixing the powder obtained through ball milling with copper chromite black in a ball milling mode. The maximum particle size of the bismuth-oxide-based black pigment is smaller than 2 micrometers, the sintering temperature on glass is between 600 DEG C and 700 DEG C, the bonding strength between the bismuth-oxide-based black pigment and the glass is high, and the bismuth-oxide-based black pigment has wide application prospects in the field of digital inkjet printing.

Description

technical field [0001] The invention belongs to the technical field of glass digital inkjet printing, and in particular relates to a bismuth oxide-based black colorant for glass digital inkjet printing and a preparation method thereof. Background technique [0002] Glass digital inkjet printing technology, as a new non-contact, pressure-free, and plate-free printing technology, pushes the development trend of glass fashion, personalization, art, small batches, multi-color, low-carbon and environmental protection to a new level. a new height. Since my country introduced the first glass inkjet machine in 2009, the development of glass digital inkjet printing technology has advanced by leaps and bounds and has been widely used. Compared with the traditional glass surface printing technology, glass digital inkjet printing technology has the advantages of lifelike, delicate and clear product patterns, quick realization of personalized design and manufacturing, and high degree of...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D11/037
Inventor 许晓静朱金鑫丁清庞伟吉顺青叶书兵
Owner JIANGSU UNIV
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