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Transformer deteriorated oil adsorbent and preparation method thereof

A degraded oil and adsorbent technology, applied in chemical instruments and methods, inorganic chemistry, silicon compounds, etc., can solve problems such as inability to handle and utilize, produce acid residue and alkali residue, and hidden dangers to operator safety, and achieve better adsorption effect Good, low cost, and the effect of improving the adsorption effect

Inactive Publication Date: 2015-11-04
STATE GRID SHANDONG ELECTRIC POWER +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The more common processing method in the prior art is to adopt H 2 SO 4 - The clay method and the acid-alkali-clay method are used to adsorb transformer oil, but there are mainly the following defects: liquid chemical materials such as acid and alkali are used in the treatment process, which has potential safety hazards for the operator and will produce some Acid slag and alkali slag cannot be treated and utilized, causing great pressure on the environment

Method used

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  • Transformer deteriorated oil adsorbent and preparation method thereof
  • Transformer deteriorated oil adsorbent and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] An adsorbent for degraded transformer oil comprises the following effective components in parts by weight: 30 parts of aluminum oxide, 40 parts of sodium silicate and 30 parts of aluminum chloride.

[0021] The raw material alumina powder, sodium silicate powder and aluminum chloride powder plus mass fraction of 40% sulfuric acid are mixed evenly, and the mixture obtained in (1) is made into particles with a particle diameter of 2 mm by a molding machine; then the particles are placed Bake in an oven at 70°C for 2 hours; then quickly raise the temperature to 700°C, and dry for 1 hour to obtain the finished product of adsorbent particles 3, the specific surface area of ​​the prepared particles is 256m 2 / g.

[0022] When in use, put the finished product of the adsorbent particle 3 in the transformer oil to absorb it by natural sedimentation, and keep the temperature of the transformer oil at a relatively high temperature, such as 60°C, during the adsorption.

Embodiment 2

[0024] This embodiment is the same as Embodiment 1 except the following features:

[0025] An adsorbent for degraded transformer oil comprises the following effective components in parts by weight: 40 parts of aluminum oxide, 30 parts of sodium silicate and 25 parts of aluminum chloride. Alumina, sodium silicate, aluminum chloride plus mass fraction are 25% sulfuric acid and are mixed evenly, and the mixture obtained in (1) is made into particles with a particle diameter of 3 mm by a molding machine; then the particles are placed in an oven at 70 Bake at ℃ for 2 hours; then quickly raise the temperature to 700℃, and dry for 1 hour to get the finished product of adsorbent particles 3, the specific surface area of ​​the prepared particles is 262m 2 / g.

[0026] After the finished product of adsorbent particles 3 is obtained, the adsorption filter plate is made according to the following method: the adsorption filter plate includes filter plate I1 placed on the upper layer and f...

Embodiment 3

[0028] This embodiment is the same as Embodiment 2 except the following features:

[0029] An adsorbent for degraded transformer oil comprises the following effective components in parts by weight: 35 parts of aluminum oxide, 35 parts of sodium silicate and 25 parts of aluminum chloride. Alumina, sodium silicate, aluminum chloride plus mass fraction are 30% sulfuric acid and mix uniformly, and the mixture obtained in (1) is made into particles with a particle diameter of 3 mm by a molding machine; then the particles are placed in an oven at 70 Bake at ℃ for 2 hours; then quickly raise the temperature to 700℃, and dry for 1 hour to get the finished product of adsorbent particles 3, the specific surface area of ​​the prepared particles is 252m 2 / g.

[0030] The finished adsorbent particle 3 is placed above the filter plate I1, and filter paper or filter cloth is placed above the finished adsorbent particle 3. The filter plate I1 has a pore size of 250 um, and the filter plate ...

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Abstract

The invention discloses a transformer deteriorated oil adsorbent and a preparation method thereof, and belongs to the field of solid adsorbent combinations or filtering additive combinations. The transformer deteriorated oil adsorbent is used for solving the problems that an existing adsorbent is unsafe and pollutes the environment seriously. The transformer deteriorated oil adsorbent comprises, by weight, 30-40 parts of aluminum oxide, 20-40 parts of sodium silicate and 20-30 parts of aluminum chloride. The prepared adsorbent is composed of inorganic components, nontoxic, nonflammable and free from danger like burning explosion in the waste oil treatment process; the preparation method of the adsorbent is simple, low in cost and free from environment pollution; the adsorbent has a large specific area and good adsorption and purification effects.

Description

technical field [0001] The invention belongs to the field of solid adsorbent composition or filter aid composition, and in particular relates to a transformer degraded oil adsorbent and a preparation method thereof. Background technique [0002] During the operation of the transformer, the transformer oil will be oxidized due to foreign matter pollution or the influence of high temperature, electromagnetic field, metal catalysis, etc. during the operation, and then the impurities in the oil will increase, the oil will be turbid, and finally become deteriorated waste oil. The more common processing method in the prior art is to adopt H 2 SO 4 - The clay method and the acid-alkali-clay method are used to adsorb transformer oil, but there are mainly the following defects: liquid chemical materials such as acid and alkali are used in the treatment process, which has potential safety hazards for the operator and will produce some Acid slag and alkali slag cannot be treated and ...

Claims

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Application Information

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IPC IPC(8): B01J20/08B01J20/10B01J20/02B01J20/30
Inventor 曹现民戴建强林建高成成陈星延李中凯
Owner STATE GRID SHANDONG ELECTRIC POWER
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