Preparation method of composite micro-encapsulated soybean lecithin powder for livestock breeding
A technology of soybean lecithin and composite microcapsules is applied in the fields of animal husbandry, application, animal feed, etc., and can solve the problem of not considering the nutritional effect of wall materials on breeding animals, etc.
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Embodiment 1
[0028] A preparation method for compound microencapsulated soybean lecithin powder for animal husbandry, the specific steps are as follows:
[0029] (1) Thoroughly agitate and extract the soybean lecithin oil with ethanol with a concentration of 90% (v / v), the extraction temperature is 30°C, the ratio of ethanol to soybean lecithin oil is 3:1 (ml / g), extract for 30min, and then centrifuge Separate the extract and insoluble matter, and collect the upper extract; repeat the extraction step twice. The acetone insoluble matter of the soybean lecithin oil is more than 55%, and the PC value of phosphatidylcholine is 18%. In order to achieve the purpose of fully stirring and extracting, ultrasonic assisted extraction can be used, the ultrasonic power is 100-150W, and the assisted extraction is 6-10min. The parameters of the centrifuge for centrifuging the extract and insoluble matter are set at 10000-13000 rpm for 15-25 minutes.
[0030] (2) Merge two extracts, carry out vacuum dis...
Embodiment 2
[0034] A preparation method for compound microencapsulated soybean lecithin powder for animal husbandry, the specific steps are as follows:
[0035](1) Thoroughly agitate and extract the soybean lecithin oil with ethanol with a concentration of 90% (v / v), the extraction temperature is 40°C, the ratio of ethanol to soybean lecithin oil is 3:1 (ml / g), extract for 60min, and then centrifuge Separate the extract and insoluble matter, and collect the upper extract; repeat the extraction step twice. The acetone insoluble matter of the soybean lecithin oil is more than 55%, and the PC value of phosphatidylcholine is 18%. Adding 1.5% by weight glass beads with a diameter of 0.9mm as a dispersant in the phospholipid raw material in advance can improve the viscosity characteristics of soybean lecithin oil during stirring, expand the solvent contact area, and improve the lecithin extraction effect. In order to achieve the purpose of fully stirring and extracting, ultrasonic assisted ext...
Embodiment 3
[0040] A preparation method for compound microencapsulated soybean lecithin powder for animal husbandry, the specific steps are as follows:
[0041] (1) Thoroughly agitate and extract the soybean lecithin oil with ethanol with a concentration of 90% (v / v), the extraction temperature is 35°C, the ratio of ethanol to soybean lecithin oil is 3:1 (ml / g), extract for 40min, and then centrifuge Separate the extract and insoluble matter, and collect the upper extract; repeat the extraction step twice. The acetone insoluble matter of the soybean lecithin oil is more than 55%, and the PC value of phosphatidylcholine is 18%. Adding 1% by weight glass beads with a diameter of 0.8 mm in advance as a dispersant to the phospholipid raw material can improve the viscosity characteristics of soybean lecithin oil during stirring, expand the solvent contact area, and improve the lecithin extraction effect. In order to achieve the purpose of fully stirring and extracting, ultrasonic assisted ext...
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