Efficient compound iron-based phosphorous-removing adsorbent as well as preparation method, application method and regeneration method thereof
A phosphorus adsorbent, iron-based technology, applied in the direction of separation methods, filter regeneration, chemical instruments and methods, etc., can solve the problems that the phosphorus in the effluent is difficult to meet the standard, and the effect does not meet expectations, etc., and achieve fast adsorption speed and simple method , the effect of excellent adsorption performance
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Embodiment 1
[0033] The preparation method of the high-efficiency composite iron-based phosphorus removal adsorbent of this embodiment is carried out according to the following steps:
[0034] One, prepare iron salt solution, ferrous salt solution, lanthanum salt solution and lye respectively;
[0035] 2. Fully mix the iron salt solution, ferrous salt solution, lanthanum salt solution and alkali solution prepared in step 1 under the conditions of aeration and stirring and a 60°C water bath, and continue aeration and stirring for 4 hours;
[0036] 3. Add diatomaceous earth and shake for 4 hours, let it stand for 12 hours for aging, discard the supernatant, and wash the solid with water until the pH of the cleaning solution is 7.3;
[0037] 4. Dry the cleaned solid in step 3 at 62° C. for 2 hours, then raise the temperature to 102° C. and keep it for 14 hours for drying to obtain a high-efficiency composite iron-based dephosphorization adsorbent.
Embodiment 2
[0039] The preparation method of the high-efficiency composite iron-based phosphorus removal adsorbent of this embodiment is carried out according to the following steps:
[0040] One, prepare iron salt solution, ferrous salt solution, lanthanum salt solution and lye respectively;
[0041] 2. Fully mix the iron salt solution, ferrous salt solution, lanthanum salt solution and alkali solution prepared in step 1 under the conditions of aeration and stirring and a 90°C water bath, and continue aeration and stirring for 2 hours;
[0042] 3. Add diatomaceous earth and shake for 3 hours, let it stand for 24 hours for aging, discard the supernatant, and wash the solid with water until the pH of the cleaning solution is 7.8;
[0043] 4. Dry the cleaned solid in step 3 at 75°C for 7h, then raise the temperature to 100°C and keep it for 24h for drying to obtain a high-efficiency composite iron-based dephosphorization adsorbent.
Embodiment 3
[0045] The preparation method of the high-efficiency composite iron-based phosphorus removal adsorbent of this embodiment is carried out according to the following steps:
[0046] One, prepare iron salt solution, ferrous salt solution, lanthanum salt solution and lye respectively;
[0047] 2. Fully mix the iron salt solution, ferrous salt solution, lanthanum salt solution and alkali solution prepared in step 1 under the conditions of aeration and stirring and a 75°C water bath, and continue aeration and stirring for 6 hours;
[0048] 3. Add diatomaceous earth and shake for 2 hours, let it stand for 2 hours for aging, discard the supernatant, and wash the solid with water until the pH of the cleaning solution is 6.8;
[0049] 4. Dry the cleaned solid in step 3 at 50° C. for 12 hours, then raise the temperature to 105° C. and keep it for 2 hours for drying to obtain a high-efficiency composite iron-based dephosphorization adsorbent.
[0050] The concentrations of iron salt solu...
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