A preparing method of an antifungal natural active substance
A natural active substance and antifungal technology, applied in botany equipment and methods, antifungal agents, chemicals for biological control, etc., can solve flammability, unsafe storage, transportation and use, low effective utilization rate, etc. problems, to achieve the effect of easy maintenance and cleaning, avoiding heat-labile components, and rapid and complete extraction
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Embodiment 1
[0032] (1) Grinding and mixing: Grind the dry matter of Xiaoguanxun, Ledang Zanthoxylum bungeanum, and Wedelia twins into coarse powder, pass through a 20-mesh sieve, and then mix according to the weight ratio of 2:2:1. (2) Extraction: put the dried Xiaoguanxun, Ledang Zanthoxylum bungeanum, and Wedelia twins in the container of the crushing extractor, add 95% aqueous ethanol equivalent to 8 times the weight ratio of the raw materials, and carry out tissue crushing and extraction at room temperature twice , the extraction time is 3 minutes. (3) Flash concentration: Suction filter the extract, discard the filter residue, and flash concentrate the obtained extract to 1 / 6 of the original volume by using a vacuum thin film concentration device below 70°C. (4) Preparation of ether extraction part: disperse the concentrated solution into water, the amount of water used is one-third of the volume of the concentrated solution. Extract with diethyl ether for 3 times, the amount of eac...
Embodiment 2
[0034] (1) Grinding and mixing: Grind the dry matter of Xiaoguanxun, Ledang Zanthoxylum bungeanum, and Wedelia twins into coarse powder, pass through a 20-mesh sieve, and then mix according to the weight ratio of 2:2:1. (2) Extraction: Put the dried Xiaoguanxun, Ledang Zanthoxylum bungeanum, and Wedelia twins in the container of the crushing extractor, add 95% aqueous ethanol equivalent to 6 times the weight ratio of raw materials, and carry out tissue crushing and extraction at room temperature for 3 times , the extraction time is 2 minutes. (3) Flash concentration: Suction filter the extract, discard the filter residue, and flash concentrate the obtained extract to 1 / 6 of the original volume by using a vacuum thin film concentration device below 70°C. (4) Preparation of ether extraction part: disperse the concentrated solution into water, the amount of water used is one-third of the volume of the concentrated solution. Extract with diethyl ether 4 times, the amount of each ...
Embodiment 3
[0036] (1) Grinding and mixing: Grind the dry matter of Xiaoguanxun, Ledang Zanthoxylum bungeanum, and Wedelia twins into coarse powder, pass through a 20-mesh sieve, and then mix according to the weight ratio of 2:2:1. (2) Extraction: Put the dried Xiaoguanxun, Ledang Zanthoxylum bungeanum, and Wedelia twins in the container of the broken extractor, add 95% aqueous ethanol equivalent to 10 times the weight ratio of the raw materials, and carry out tissue crushing and extraction at room temperature twice , the extraction time is 3 minutes. (3) Flash concentration: Suction filter the extract, discard the filter residue, and use a vacuum thin-film concentration device to flash-concentrate the obtained extract below 70°C to 1 / 7 of its original volume. (4) Preparation of ether extraction part: disperse the concentrated solution into water, the amount of water used is one-third of the volume of the concentrated solution. Extract with diethyl ether 5 times, the amount of each time ...
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