Surface-modified aramid fiber and preparation method thereof
An aramid fiber and surface modification technology, applied in the field of organic fibers and their preparation, can solve the problems of large surface inertness and poor UV resistance, and achieve the effects of improving UV resistance, low cost, and improving flame retardant properties
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Embodiment 1
[0027] 1. Preparation of surface modified aramid fiber
[0028] (1) 0.5g para-aramid fiber (Kevlar-49, diameter 12um, density 1.43g / cm 3 , produced by DuPont Company of the United States) were immersed in acetone, petroleum ether, and deionized water in turn, and each was refluxed for 3 hours; after cleaning, the fibers were taken out and dried at 80°C for 12 hours to obtain clean aramid fibers, which were denoted as KF . Its infrared spectrum is attached figure 1 , surface contact angle and free energy are shown in Table 1.
[0029] (2) Stir and dissolve 10.5g of sodium hydroxide in 120mL of ethanol to obtain an ethanol solution of sodium hydroxide; immerse 0.1g of the KF fiber obtained in step (1) into the ethanol solution of sodium hydroxide, and reflux for 5 hours; After the reaction is finished, the fibers are washed with water and dried to obtain fibers with amino groups on the surface.
[0030] (3) Under the protection of nitrogen atmosphere, take 0.1g of aramid ...
Embodiment 2
[0041] 1. Preparation of surface modified aramid fiber
[0042] (1) Stir and dissolve 10.5g of sodium hydroxide in 120mL of ethanol to obtain an ethanol solution of sodium hydroxide; immerse 0.1g of the clean fiber KF obtained in step (1) of Example 1 into the ethanol solution of sodium hydroxide, Reflux for 5 hours; after the reaction, wash with water and dry to obtain fibers with amino groups on the surface.
[0043] (2) Under the protection of a nitrogen atmosphere, take 0.1g of the aramid fiber with amino groups obtained in step (2), add 30mL of γ-glycidyl etheroxypropyl trimethoxysilane, and 150mL of absolute ethanol solvent into a 250mL three-necked flask, and place at 70°C Under reflux for 12 hours, aramid fibers with methoxy groups on the surface were obtained.
[0044] (3) Dissolve 14.9g of cerium chloride and 1.11g of calcium chloride in 150mL of deionized water to obtain a mixed solution of cerium chloride and calcium chloride; add 6g of sodium hydroxide to the mix...
Embodiment 3
[0051] 1. Preparation of surface modified aramid fiber
[0052] (1) Stir and dissolve 10.5g of sodium hydroxide in 120mL of ethanol to obtain an ethanol solution of sodium hydroxide; immerse 0.1g of the clean fiber KF obtained in step (1) of Example 1 into the ethanol solution of sodium hydroxide, Reflux for 5 hours; after the reaction, wash with water and dry to obtain fibers with amino groups on the surface.
[0053] (2) Under the protection of a nitrogen atmosphere, take 0.1g of the aramid fiber with amino groups obtained in step (2), add 30mL of γ-glycidyl etheroxypropyl trimethoxysilane, and 150mL of absolute ethanol solvent into a 250mL three-necked flask, and place at 70°C Under reflux for 12 hours, aramid fibers with methoxy groups on the surface were obtained.
[0054] (3) Dissolve 14.9g of cerium chloride and 1.11g of calcium chloride in 150mL of deionized water to obtain a mixed solution of cerium chloride and calcium chloride; add 6g of sodium hydroxide to the mixed...
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