A production method for preparing calcium dihydroxide phosphate special fertilizer for peony by-product
A production method and technology of calcium hydroxide, applied in chemical instruments and methods, phosphorus compounds, applications, etc., can solve the problems of soil compaction, stagnation, slowing down of peony growth, etc., achieving good controllable release, large number of flower buds, Good absorption rate
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Embodiment 1
[0064] The production method for preparing special fertilizer for peony by-product of potassium dihydrogen phosphate provided in this embodiment mainly includes the following steps:
[0065] 1) Mix phosphoric acid and carbamide according to the molar ratio of 1.2:1, and raise the temperature from 80°C to 160°C at a heating rate of 6°C / min, stir and react for 4-5h, and separate the intermediate; then use the intermediate with The alkaline potassium salt is mixed according to the molar ratio of 1:1.4, and the pH is adjusted to 8.5-9.0. After the reaction is completed, a slurry containing nitrogen, phosphorus, and potassium is obtained, and the slurry containing nitrogen, phosphorus, and potassium is cooled Cool down the temperature in the crystallizer to 35-40°C, perform crystallization filtration treatment, make the filtrate circulate and crystallize in the cooling crystallizer, the filter cake obtained is potassium dihydrogen phosphate product, and the content of the components in...
Embodiment 2
[0075] The production method for preparing special fertilizer for peony by-product of potassium dihydrogen phosphate provided in this embodiment mainly includes the following steps:
[0076] 1) Phosphoric acid and carbamide are mixed according to the molar ratio of 1.5:1, and the temperature is raised from 80 to 160 at a heating rate of 6°C / min, and the reaction is stirred for 4-5h to obtain the intermediate; then the intermediate is used with The alkaline potassium salt is mixed according to the molar ratio of 1:1.1, and the pH is adjusted to 8.5-9.0. After the reaction, a slurry containing nitrogen, phosphorus, and potassium is obtained, and the slurry containing nitrogen, phosphorus, and potassium is placed in cooling The temperature in the crystallizer is lowered to 35-40°C, and the crystallization filtration treatment is carried out. The filtrate is circulated and crystallized in the cooling crystallizer. The filter cake obtained is potassium dihydrogen phosphate product. The...
Embodiment 3
[0086] The production method for preparing special fertilizer for peony by-product of potassium dihydrogen phosphate provided in this embodiment mainly includes the following steps:
[0087] 1) Mix phosphoric acid and carbamide in a molar ratio of 1.3:1, and raise the temperature from 80°C to 160°C at a heating rate of 6°C / min, stir and react for 4-5h, and separate the intermediate; then use the intermediate with The alkaline potassium salt is mixed according to the molar ratio of 1:1.3, and the pH is adjusted to 8.5-9.0. After the reaction is completed, a slurry containing nitrogen, phosphorus, and potassium is obtained, and the slurry containing nitrogen, phosphorus, and potassium is cooled The temperature in the crystallizer is lowered to 35-40°C, and the crystallization filtration treatment is carried out. The filtrate is circulated and crystallized in the cooling crystallizer. The filter cake obtained is potassium dihydrogen phosphate product. The content of the components in...
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