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Preparation method of poly(phenol-amine) superhydrophilic particulates

A super-hydrophilic and polyphenolamine technology, which is applied in the treatment of fibrous fillers, coatings, and dyed polymer organic compounds, can solve the problems of difficult preparation of super-hydrophilic surfaces, complex precision instruments and equipment, and harsh preparation conditions. Achieve good superhydrophilic performance, controllable process and low cost

Inactive Publication Date: 2015-01-07
QILU UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But as far as the current research status is concerned, there are still a series of problems to be solved: (1) the current preparation process is limited to the preparation of small-area super-hydrophilic surfaces, and there are still difficulties in the preparation of large-area super-hydrophilic surfaces; (2) some The preparation method of super-hydrophilic surface is cumbersome, and the preparation conditions are harsh, and the manufacturing cost is high; (3) Some preparation methods of super-hydrophilic surface require complex and sophisticated instruments and equipment, which are expensive and take a long time

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] Add polytetrafluoroethylene (PTFE) particles with a particle size of 2-5 μm to the ethanol solution of catechol and hexamethylenediamine at a concentration of 0.3mol / L, react for 24 hours under magnetic stirrer stirring, and then centrifuge; The prepared PCAPTFE microparticles are vacuum-dried at 40° C. to obtain polyphenolamine microparticles with superhydrophilic properties.

Embodiment 2

[0020] Add polystyrene microspheres (PS microspheres) with a particle size of 1 μm to an aqueous solution of hydroquinone and triethylenetetramine at a concentration of 0.1 mol / L, react for 36 hours under stirring with a magnetic stirrer, and then centrifuge; That is, PCAPS polyphenolamine microparticles with superhydrophilic properties are obtained.

Embodiment 3

[0022] Add multi-walled carbon nanotubes (CNTs) with a length of 5-15 μm and a diameter of 20-40 nm to an aqueous solution of catechol and diethylenetriamine at a concentration of 0.2 mol / L, react for 12 hours under magnetic stirrer stirring, and centrifuge ; That is, PCACNTs polyphenolamine particles with superhydrophilic properties are obtained.

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Abstract

The invention discloses a preparation method of poly(phenol-amine) superhydrophilic particulates. The preparation method of the poly(phenol-amine) superhydrophilic particulates comprises the following steps: firstly adding a micro-nano material into a solution of polyphenol and polyamine, reacting for a period of time, and separating, so that the superhydrophilic particulates are obtained. The preparation method of the poly(phenol-amine) superhydrophilic particulates is simple in process, easy to operate, controllable in technology, mild in conditions, good in repeatability, low in cost and convenient for popularization and application, the obtained poly(phenol-amine) superhydrophilic particulates have good superhydrophilic performance, can be applied to various materials and have a broad application range.

Description

technical field [0001] The invention relates to the field of surface modification of materials and compounding of organic and inorganic materials, in particular to a method for preparing superhydrophilic materials by using polyphenolamines to modify micro-nano materials. Background technique [0002] Wettability is one of the important properties of a solid surface, and the contact angle (CA) is usually used to characterize the wettability of a liquid to a solid. The wettability of solid surfaces is very important for basic research and practical applications. In recent years, superhydrophilic and superhydrophobic surfaces have attracted extensive attention as a very special phenomenon. Super-hydrophilic surface refers to the surface with a contact angle of less than 5° with water. It has important characteristics such as self-cleaning, anti-fog, and improved surface heat exchange efficiency. It can be widely used in many fields such as scientific research, production, and l...

Claims

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Application Information

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IPC IPC(8): C08J7/04C08J7/00C08L27/18C08L25/06C08L79/02C08G73/02C09C1/44C09C1/28C09C3/10
Inventor 刘钦泽周广盖姚金水刘伟良乔从德
Owner QILU UNIV OF TECH
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