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Method for improving plasticity and flexibility of bacterial cellulose membrane

A technology of bacterial cellulose membrane and bacterial cellulose, applied in the fields of polymer chemistry and polymers, can solve the problems of lack of flexibility and plasticity of bacterial cellulose membrane

Active Publication Date: 2015-01-07
TIANJIN UNIVERSITY OF SCIENCE AND TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
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Problems solved by technology

[0005] The problem to be solved by the present invention is the lack of flexibility and plasticity of bacterial cellulose membrane in application, so a simple and economical composite method is proposed to improve the flexibility of bacterial cellulose and expand the application of bacterial cellulose range; Secondly, for the toughening agent polyetheramine, the cost of polyetheramine is low, the toxicity is small, and the pollution to the environment is small, so it is a better toughening agent in the modification of bacterial cellulose

Method used

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  • Method for improving plasticity and flexibility of bacterial cellulose membrane

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Embodiment Construction

[0020] In the present invention, after the bacterial cellulose membrane is fermented, synthesized and purified, it is not dried and then combined with the wet membrane. Compared with the previous composite of the dry membrane, because the water holding rate of the bacterial cellulose membrane can reach 99%, it is suitable for The compounding of the wet film can make the toughening agent penetrate into the three-dimensional network structure of the bacterial cellulose film better and more; the invention is carried out under normal temperature and pressure, which reduces the operating cost and has less environmental pollution.

[0021] Take bacterial cellulose / polyetheramine D230 composite as an example:

[0022] 1) Preparation of cellulose membrane

[0023] Pick 1~3 rings of G.xylinum bacteria from the slope under sterile conditions and inoculate them into the Erlenmeyer flasks filled with 100mL of sterilized medium, and place them in a shaker incubator at 30°C and 180rpm Unde...

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Abstract

The invention relates to a method for improving the plasticity and flexibility of a bacterial cellulose membrane. Microbial Gluconacetobacter xylinum is cultured by static culture so as to obtain an initial bacterial cellulose wet membrane sample, and after the sample is soaked in alkaline liquor and then soaked and purified in deionized water, the purified bacterial cellulose membrane is soaked into polyether amine salt solutions with different concentrations (1-5.2wt%) firstly, the obtained object is put into an oscillator to oscillate and compound for 24h at room temperature, and then the compounded bacterial cellulose membrane / polyether amide membrane, after being washed by using deionized water, is dried at certain temperature, the plasticity of the obtained final bacterial cellulose / polyether amine compounded membrane is 45.8%, compared with the plasticity 4% of a bacterial cellulose membrane before compounding, the plasticity of the compounded cellulose membrane is increased by 11.45 times, so that the bacterial cellulose is applied more widely to the fields of chemical engineering, paper making and biomedicine; and in addition, the method is low in production and operation costs, less in equipment investment, and high in feasibility.

Description

technical field [0001] The invention belongs to the field of polymer chemistry and polymer technology, and mainly relates to a method for directly compounding bacterial cellulose wet film with polyether amine salt to improve the plasticity and flexibility of bacterial cellulose. technical background [0002] Bacterial Cellulose is a type of pure cellulose produced by microorganisms. From the molecular composition of cellulose, both are directly composed of β-D-glucose through β-1,4-glucosidic bonds. The straight chains are parallel to each other, not in a helical conformation, and without branched structure, also known as β-1,4-glucan. Bacterial cellulose is chemically identical to cellulose produced by plants or algae. However, as a new type of biological material, bacterial cellulose has many unique properties. 1) High crystallinity and high chemical purity. It does not contain hemicellulose, lignin and other cell wall components, and the purification process is simple;...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08J7/00C08L1/02C08L71/00C12P19/04C12R1/01
Inventor 钟成张玉明贾士儒谭之磊韩培培乔长晟
Owner TIANJIN UNIVERSITY OF SCIENCE AND TECHNOLOGY
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