Multifunctional high-performance carbon-based nanoparticle/sodium alginate composite fibers and preparation method thereof
A sodium alginate and composite fiber technology, applied in the chemical characteristics of fibers, alginate rayon, rayon manufacturing and other directions, can solve the problems of decreased fiber elongation at break, modified algae fibers, poor fiber toughness, etc. , to achieve the effect of excellent tensile strength
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Embodiment 1
[0023] a. Add sodium alginate to water, stir at room temperature for 0.5 hours, then stir at 35°C for 2 hours, and configure a sodium alginate aqueous solution with a concentration of 3% by mass;
[0024] b. adding graphene oxide to the sodium alginate aqueous solution obtained in step a, so that the mass percentage concentration of graphene oxide is 1%, and then adopt ultrasonic treatment for 2 hours to obtain graphene oxide / sodium alginate aqueous solution;
[0025] c. Add carbon nanotubes to the graphene oxide / sodium alginate aqueous solution obtained in step b, so that the mass percent concentration of carbon nanotubes is 0.01%, and then use ultrasonic treatment for 0.5 hours to obtain carbon nanotubes / graphene oxide / Sodium alginate spinning solution;
[0026] d. Place the carbon nanotube / graphene oxide / sodium alginate spinning solution obtained in step c in a vacuum oven for 6 hours for defoaming until the mixed solution has no bubbles;
[0027] e. The carbon nanotube / ...
Embodiment 2
[0031] a. Add sodium alginate to water, stir at room temperature for 5 hours, then stir at 50°C for 5 hours, and configure a sodium alginate aqueous solution with a concentration of 15% by mass;
[0032] b. adding graphene oxide to the sodium alginate aqueous solution obtained in step a, so that the mass percentage concentration of graphene oxide is 0.01%, and then adopt ultrasonic treatment for 2 hours to obtain graphene oxide / sodium alginate aqueous solution;
[0033] c. Add carbon nanotubes to the graphene oxide / sodium alginate aqueous solution obtained in step b, so that the mass percentage concentration of carbon nanotubes is 1%, and then use ultrasonic treatment for 0.5 hours to obtain carbon nanotubes / graphene oxide / Sodium alginate spinning solution;
[0034] d. Place the carbon nanotube / graphene oxide / sodium alginate spinning solution obtained in step c in a vacuum oven for 24 hours for defoaming until the mixed solution has no bubbles;
[0035] e. The carbon nanotub...
Embodiment 3
[0038] a. Add sodium alginate to water, stir at room temperature for 5 hours, then stir at 60°C for 5 hours, and prepare an aqueous solution of sodium alginate with a concentration of 20% by mass;
[0039] b. adding graphene oxide to the sodium alginate aqueous solution obtained in step a, so that the mass percentage concentration of graphene oxide is 1%, and then adopt ultrasonic treatment for 2 hours to obtain graphene oxide / sodium alginate aqueous solution;
[0040] c. Add carbon nanotubes to the graphene oxide / sodium alginate aqueous solution obtained in step b, so that the mass percent concentration of carbon nanotubes is 0.01%, and then use ultrasonic treatment for 0.5 hours to obtain carbon nanotubes / graphene oxide / Sodium alginate spinning solution;
[0041] d. Place the carbon nanotube / graphene oxide / sodium alginate spinning solution obtained in step c in a vacuum oven for 24 hours for defoaming until the mixed solution has no bubbles;
[0042]e. The carbon nanotube / ...
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